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GCMS analysis results for sample AE01638, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010126–000010145

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . • Data File : C: \MSDCHEM\1\5973N\02FEB21\01638.D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.62 ug/L 516072 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-D10 188 C14D10 000000-00-0 50 3 1,2-Bis(2-hydroxyphenyl)ethylene. .. 376 C24H28N2O2 000000-00-0 38 4 1-acetyl-3-oxo-4-phenyl-3-butene 188 C12H1202 000000-00-0 38 Abundance Scan 1718 (22.768 min): 01638.D (-) m/z 188.10 100.00% 188

5000

43 57 66 80 94 108 132 146 160 | --------- 1 22.40 22.60 22.80 23.00 0- mp — -* ‘‘1‘1 m/z 189.10 23.37% niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 80 94 m/z 94.00 19.59% 66 158

miz-> 0- IT I I I ■ [ I . > I | I 1 ! I | 11 ! ■ ooIf mpTmP 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 slaani Abundance #84498: Anthracene-D10 188 ■ i ' 1 1 ■ i 1 ■ 1 1 i ■ ■ • ' I ■ 1 ■ ■ i ■ 22.40 22.60 22.80 23.00 5000 m/z 80.05 16.95% 80 94 66 160 ,|

miz-> O—mTTT -H TT, mmmmm-mmdmm 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #318194:1,2-Bis(2-hydroxyphenyl)ethylenediamine, N,N’-bis... .......... ............................... 188 22.40 22.60 22.80 23.00 m/z 92.00 15.36%

5000

94 107 121 139 145 172

m/z-> 0- " i'1 ‘ ■ i •" ■ i ■ “ ■ i ■ ■ 40 50 60 70 80 ■I 80 “ i1 131116117 —4ll 90 100 110 120 130 140 150 160 170 180 190 ........... / . । ............ ............. । . .-I । ******* I * 22.40 22.60 22.80 23.00

01638.D HP022102.M Mon Feb 25 10:55:51 2002 Page 13

NYC-WTC_000010142

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NYC-WTC_000010142Source: NYC Law Department, mirrored locally

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