GCMS analysis results for sample AD31673, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31673 including unknown compounds and surrogate recovery data.

NYC-WTC_000050053–000050065

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document ulbrary searor compound xeporc

Data File : C:\MSDCHEM\1\5973N\02JAN17\31673 .D Vial: 8 • Acq On : 17 Jan 2002 8:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to’ ISTD R.T. 5.89 4.94 ug/L 1627690 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-... 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 220 (5.885 min): 31673.D (-) m/z 73.10 100.00% 73

5000 43 * *′1′11*1′44* 11.4 । i । । i । ।

ufe-> 0- mm 55 ., 87 103 -ppp ■ r-1 • • ■ ■ i “ i “ “ i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1 ■i•“•i‘ •i “ i “ “ i “ *11 ■ m/z 5.60 5.80 43.10 6.00 6.20 23.05% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ' 5.60 5.80 6.00 6.20 43 m/z 41.10 8.73% 27 miz-> 0- •1 r “' i ■ “ ■ i1 mmmm , , 55 i 87 113 174 '1111 >. i'. ।.... P... (ri., ।. ■., ।.... ।.,.. ।.... ।.... । > i. > ।. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 34[1,3]dioxolan-2-ylpropyl ester 70 IImIa’ if'! i । ■ | । l . ' 5.60 5.80 ।6.00 6.20 5000 m/z 45.10। 8.72% 43 27 55 , 87 113 174 0-Tpp ■ i • ■ “ i ‘ “ ‘i1• 11n—udu——m"n9dmn—mmmIIATI n/z-> 10 20 30 40 50 60 70 80 90 1(X) 110 1M 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ' ' ■ ■ i 1 ■ • i ’ ■ 1 ■ 30 5.60 6.20 73 m/ z 6.46%

5000 44 58 15

m/z-> 0J 7 ——— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1 11 0*1 5.60 5.80 6.00 6.20

31673.D SCAN508.M Tue Jan 22 08:37:34 2002 Page 6

NYC-WTC_000050062

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GCMS analysis results for sample AD31631, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049916

Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.

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