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GCMS analysis results for sample AE01507, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009946–000009965

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\5973N\02FEB21\01506 .D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2-CYANOCARBAZOLE $$ 9H-Carb. . . Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.15 ug/L 108829 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H1203 000607-91-0 53 4 1-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 083415-88-7 50 Abundance Scan 1675 (22.283 min): 01506.D (-) m/z 192.00 100.00% 152

5000 -------- 96 146 160 22.00 22.20 22.40 22.60

niz—> 0 41 49 57 70 82 —m 120 HTTTTTTTT . ■ .-Li. ..J...., 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll. m/z 193.10 16.49% Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 102

5000 1 ■ ■ i ■ ■ ■ ■ i ■ ' ■ 1 i • ■ ■ ■ i ■ 1 ■ ■ 22.00 22.20 22.40 22.60 m/z 96.00 16.38% 164

miz—> 96 0 -rrpnn-rpn-rTjTTTTp-rTnyTTn-TTTTTTp-rrTpr^^ 138 —hmPmamp b 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1“ —l Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 19 2

22.00 22.20 22.40 22.60 5000 m/z 191.10 15.43%

96 164 138 0 ‘1—***t**4*1-***/****1****2** qmmm n/z-> 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 ...................... ............ ...... Abundance #102624: 1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)- (CAS)... 192 22.00 22.20 22.40 22.60 m/z 146.10 13.09% 5000

91 165 119 131 i47

iz-> I 103 0 mOmPmpmmmmm .. ।....I ।. 1** I II **,****,****1*81*4 +p 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Xu 22.00 22.20 22.40 22.60

01506.D HP022102.M Mon Feb 25 10:54:45 2002 Page 13

NYC-WTC_000009962

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