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GCMS analysis results for sample AE01507, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009946–000009965

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02FEB21\01506.D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.94 ug/L 689309 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 80 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 Anthracene-D10 188 C14D10 000000-00-0 56 4 Phenanthrene-diO 188 C14D10 001517-22-2 56 Abundance Scan 1718 (22.768 min): 01506.D (-) m/z 188.10 100.00% 188

5000

80 94 • i ' ■ ITt I IIIIIIII 49 66 . 102 136 146 160 22.40 22.60 22.80 23.00 I I 4 I 1 1 I |'l < I | I r rr| 11 I I | I > ! I 11 11 I | > I I I | I I I'l | 1 I > ! | I ——— m/z 80.00 21.12% 0- niphade H "i ■ i' nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 80 94 m/Z 94.00 19.51%

niz—> 66 0- 111111111 ■" ■ i'11' i ■ T-rr TTn wmPT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 L Abundance #84502: Anthracene-d10- 188 . —- . 22.40 22.60 22.80 23.00 5000 m/z 189.10 10.94%

miz-> 01 Abundance —s. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #84498: Anthracene-D10 160 , ,

1118 22.40 22.60 22.80 23.00 m/z 160.00 8.94%

5000 80 94 66 160 1 miz—> 0 q ‘IF mmHH 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Vttt ■ | • • » • | . I ■ • • • l • . • • | • 22.40 22.60 22.80 23.00

01506.D HP022102.M Mon Feb 25 10:54:45 2002 Page 14

NYC-WTC_000009963

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NYC-WTC_000009963Source: NYC Law Department, mirrored locally

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