GCMS analysis results for sample AE02721, March 5 2002

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Library Search Compound Report

’• Data File : C:\MSDCHEM\l\5973N\02FEB28\02721 .D vial: 6 Acq On : 28 Feb 2002 6:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.45 ug/L 301511 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-D10 188 C14D10 000000-00-0 87 3 Phenanthrene-dlO 188 C14D10 001517-22-2 72 4 Anthracene-dlO- 188 C14D10 001719-06-8 64 Abundance Scan 1718 (22.768 min): 02721.D (-) m/z 188.10 100.00% 188

5000 80 94 _________ ______ ______________ ‘ I ' ‘ ‘ I ' , r' I । । | ri i > | । 52 66 132 146 159 22.40 22.60 22.80 23.00

niz-> 0- - ■I "I.... Ilapla mPmmPmmm !‘s 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 25.72% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 ' I ' ‘ ‘ ■ 1 ' • •’1'1 1 T1’ 1 1 1 1 ′′ 22.40 22.60 22.80 23.00 80 94 m/z 80.05 24.61% 66 158 0- ■ i • < * * । ■ I. । ■ * । — i"1H11" i" i ■ *■ ■ i T‘ T miz-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 '' 1 ' 5000 m/z 184.00 17.07% 80 94 66 160 0- 1111 50 aislaganna 60 70 -r-n-rf 80 mmmmRH 90 1(X) 110 120 130 140 150 160 170 180 190 ll. Abundance #84499: Phenanthrene-d10 . H ; . . ■ ] i i r i । r■

188 22.40 22.60 22.80 23.00 m/z 189.10 16.00%

5000-

80 94 160 66 0 '111 ‘ " 1111' i " 1 .... Ill....... ’W.... iz-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

02721.D HP022102.M Fri Mar 01 10:07:53 2002 Page 13

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