GCMS analysis results for sample AE02721, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report *• Data File: C: \MSDCHEM\1\5973N\02FEB28\02721.D Vial: 6 Acq On : 28 Feb 2002 6:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Dibutyl phthalate Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.10 ug/L 66389 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate 278 C16H2204 000084-74-2 74 2 Phthalic acid, butyl ester, este... 336 C18H24O6 000085-70-1 74 3 1,2-Benzenedicarboxylic acid, bi... 278 C16H2204 000084-69-5 74 4 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 74 Abundance Scan 1903 (24.857 min): 02721 .D (-) m/z 149.00 100.00% 149

5000

41 56 76 104 205 223 24.60 24.80 25.00 25.20 0 pptnrni I* । ■ । ■ i । > । > । 11 । । > । ■ i । । । । ■ ■ i ' ■' ■ i ' ■ • ■ i ■ ■ ■ ■ i ‘ 1 • ■ i ■ ■ ■ • i' ■ ■ • i ■ m/z 150.00 11.38% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223244: Dibutyl phthalate 149

5000 T T 24.60 24.80 25.00 25.20 m/z 41.10 5.46%

mz-> 40 OTTt , 76 93 104 121 57 4*pondipBus 60 205 223 r fi i., ।।j— 80 100 120 140 160 180 200 220 240 260 280 274 A Abundance #286375: Phthalic acid, butyl ester, ester with butyl glyc... 149 ' ■ i ■ 1 ■ ■ I' ■ ■ i ■ ■ ‘ ' i • ■ 24.60 24.80 25.00 25.20 5000 m/z 104.00 5.26%

57 76 93104 121 167 295 223 278 0-anaaddalpoua h . H | J ■ ■ I ■ ■''i■1■■i■■■•।।■■ > । ■ ■ ■ 1 i' 1 ■ ‘i ■ mfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223251:1,2-Benzenedicarboxylicacid, bis(2-methylpropyl)... 149 24.60 24.80 25.00 25.20 m/z 56.10 4.28%

5000

57 I 76 93104 121 205 223 167 OTIT PP-m 1236 ■ ■ i 1 1 ‘ • i ‘ ■ 278 /z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

02721.D HP022102.M Fri Mar 01 10:07:53 2002 Page 14

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