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← Document results/DEP Box 14/GCMS X 2/5/02 A 2/28/02
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GCMS analysis results for sample AE02720, March 5 2002

Machine-extracted title · confidence 50%

Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02720 including surrogate recovery.

NYC-WTC_000011027–000011045

Folder label: “GCMS X 2/5/02 A 2/28/02”

←Page 14 of 19→
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NYC 9/11 Public Portal Document

Library Search Compound Report : C:\MSDCHEM\1\5973N\02FEB28\02720.D . . Data File Vial: 5 Acq On : 28 Feb 2002 6:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 101679 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 64 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 64 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 59 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 Abundance Scan 1675 (22.283 min): 02720.D (-) m/z 192.00 100.00% 1912

5000

. 96 146 ■ ■ । ■ ■ ■ ■ । 160 22.00 22.20 22.40 22.60 49 70 82 1 118 01 PT mm i' >'<’■mppemprm m/z 146.10 16.77% m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS fl 19/2

A / 5000 T 1**1 I * ' 22.00 22.20 22.40 22.60 96 164 m/z 193.00 15.80% 138

niz-> A 01 • i1' ■ ■ i • ■ ■ ■ i' ■ ■11 ■ ‘ • i ■ X l < < ‘ ‘ I < 1 ' < I * > < I l • »« < I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Cartjazole-2-carbonitrite (CAS 192 ■ ■ i ■ ■ ■ 1 i ■ 22.00 22.20 22.40 22.60 5000 m/z 191.00 14.73%

0- •aBaa****** TIIr 9 138 T । —............. ... ........................ niz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propeny)- (CAS)... 192 22.00 22.20 22.40 22.60 m/z 96.00 14.17%

5000

91 165 119 131 ..................1193 0 ■' i • ‘" i' ■1111'1' I" 111"'‘T ।' 11111 ’I’I .—..... 011uu 147 11 —nu I —B2dt1r 147— m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02720.D HP022102.M Fri Mar 01 10:07:42 2002 Page 10

NYC-WTC_000011040

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NYC-WTC_000011040Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

9 shared non-person entities · 1 shared topics · similarity 0.998

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