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GCMS analysis results for sample AE01507, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009946–000009965

Folder label: “GCMS X 1/23/02 A 2/21/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\5973N\02FEB21\01506 .D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1. . .\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Dodecane, 2,2,11,11-tetrame... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

21.41 0.09 ug/L 66770 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane, 2,2,11,11-tetramethyl- 226 C16H34 127204-12-0 53 2 Undecane, 3,5-dimethyl- (CAS) 184 C13H28 017312-81-1 50 3 Undecane, 3,5-dimethyl- 184 C13H28 017312-81-1 50 4 Dodecane, 2,6,10-trimethyl- 212 C15H32 003891-98-3 50 Abundance Scan 1598 (21.414 min): 01506.D (-) m/z 57.10 100.00% 57 71

5000 43 85 99 113 —l 1ffM ft, । rmmrr2 14 . 1 127 21.00 21.20 21.40 21.60 21.80 0- — .... 1 ■ i ■ “ ■ i 111 • i..... 11......7............................... ■ ■■■i11■•।■*1 ■ ।' *1 । • • ■ ■ । ■■" । ■ ■■■i"'‘।■'■> । ■ m/z 71.10 71.72% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #154955: Dodecane, 2,2,11,11-tetramethyl- 57

........................................... . 5000 21.00 21.20 21.40 21.60 21.80 m/z 43.10 38.89% 71 RR , J j 99 113 127 141 155 168 miz-> 0- .... 42., 11m0110001**puut—pamupmmunngT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93411: Undecane, 3,5-dimethyl- (CAS) 57

21.00 21.20 21.40 21.60 21.80 5000 m/z 85.10 35.13% 71

iz-> 0- '111 ■1111 ‘ ■ u i ■11 ■ i' ...7.%..422 11**8100 184 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 127 155

Abundance #93410: Undecane, 3,5-dimethyl- 57 21.00 21.20 21.40 21.60 21 .'80 m/z 56.10 26.53% 5000 71

miz-> 33 | 0 1' i1 ■" i ■ “ ■ i1 ■1' i “ 85 99 112 H 127 155 184 !‘ TP *1118 11 “ ‘ i ■ “ ■ i11 ■ ■ i ■1 “ i • ■ “ i'1 ■11 ‘ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 A 21.00 21.20 21.40 21.60 21.80

01506.D HP022102.M Mon Feb 25 10:54:45 2002 Page 12

NYC-WTC_000009961

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NYC-WTC_000009961Source: NYC Law Department, mirrored locally

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