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GCMS analysis results for sample AE00838, Feb 4 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052167–000052186

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052180
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00838.D Vial: 2 Acq On : 31 Jan 2002 3:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Dodecane (CAS) $$ n-Dodecan... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

13.41 0.15 ug/L 109247 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane (CAS) $$ n-Dodecane $$ ... 170 C12H26 000112-40-3 78 2 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 78 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 78 4 Hexadecane 226 C16H34 000544-76-3 72 Abundance Scan 879 (13.409 min): 00838.D (-) m/z 57.10 100.00% 57 43 71 5000

97 112 85 4 44AA- 13.00 13.20 13.40 13.60 13.80

Wz-> 0 ......... 'I1 n—r i. il. .... I".। 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 43.10 69.43% Abundance #74393: Dodecane (CAS) $$ n-Dodecane $$ Ba 51-090453 $$ Ad... 43 57

5000 71 13.00 13.20 13.40 13.60 13.80 85 m/z 71.10 54.15% 27

n/z-> o1 :20 4 | , *010009)0099*09——— 99 113 127 I" ” I 170 "I"... I.... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance> #113286: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57 40. 13.00 13.20 13.40 13.60 13.80 5000 71 m/z 85.10 34.25% 85 27 o1... 1..... | , 99 113 127 141 154 ■ ■ i'■ i ■ ■ il .... 11'.।1 .1।।। 198 n/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance> #113302: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane Itir 4 13.00 13.20 13.40 13.60 13.80 57 m/ z 41.10 30.18%

5000 71 85

m/z-> 0 27 - ■ ■99 113 127 198 1111 •' i r" ■ ।' i"' ■ i" " r ' ■' r "' r 1" r '1111'11 r11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 AAMws 1300 13.20 13.40 13.60 13.80

00838.D SCAN508.M Fri Feb 01 09:19:07 2002 Page 10

NYC-WTC_000052180

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NYC-WTC_000052180Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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machine-extracted · confidence unavailable · Check page ↗

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