GCMS analysis results for sample AE01508, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

* Data File : C: \MSDCHEM\1\5973N\02FEB21\01507.D Vial: 4 Acq On : 21 Feb 2002 1:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Tetradecane (CAS) $$ n-Tetr... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

21.33 0.03 ug/L 22831 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 83 2 Octane, 2,4,6-trimethyl- 156 C11H24 062016-37-9 64 3 4,4-Dimethylcyclooctene 138 C10H18 000000-00-0 59 4 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 50 Abundance Scan 1591 (21.334 min): 01507.D (-) m/z 57.10 100.00% 57 71 43 85 5000 .............. . 99 21.00 21.20 21.40 21.60 0 ■rp-r " ' ‘ l‘ " I " '"‘1 IT’ 1 1 1 ' “ I 1 1 “ I " " I “ ‘ ' I " ' ‘ I ‘‘' I |'“‘| m/z 71.10 63.85% m/z-> 2030405060 70 8090 100110120130 140150 160170180 190 200 Abundance #113295: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57

5000 71 ‘ ' I ' ' ‘ ' I ' ' ' 1 I T-r-p-r-r-r-r

85 21.00 21.20 21.40 21.60 m/z 85.10 54.50% . 99 113 127 141 155 168 411111 Pl 11111 l'l 111.1 IS 11111 l'l । > 111 l'l 11111 >'11111 > 1111 > 1|.... I... 11... 198 0 ■ i11" n/z-> 2030405060 70 8090 100110 120130140150160170180 190 200 Abundance #56276: Octane, 2,4,6-trimethyl- 57 T-Tp-TT-r-r-pr-r I ‘ ‘ ' I ' ' ‘ ' I 21.00 21.20 21.40 21.60 5000 m/z 43.10 52.01% 71 85

n/z-> 0 ........ I 99 127 I { I I I 1 I I I ( I I I I [ I I I l^| I I H | I I I I | I ! l'l [ I I I I [ I I I I j I I I I | l 1 * I | « * I > | * > । i | I i i * |

2030405060 70 8090 100110120130140150160170180190 200 Abundance #34435:4,4-DimethyIcyclooctene *I 57 21.00 21.20 21.40 21.60 43 85 m/z 55.00 30.79%

5000

27 71 99

O-pmpp 4mmp /.p.pmmmm ■ ■ i ■ 1 ■ ■ i • ■ i ■ ■ ■ ' i ■ ■ ■ ■ i miz—> 20 30 40 50 60 70 80 90 100110 120130140150160170180 190 200 21.00 21.20 21.40 21.60

01507.D HP022102.M Mon Feb 25 10:54:52 2002 Page 13

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