GCMS analysis results for sample AD31638, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31638.D Vial: 5 ' Acq On : 17 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst. . : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************** * * ******************************** Peak Number 3 1-Propanamine (CAS) $$ n-Pr... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 5.51 0.11 ug/L 35093 1,4-Dichlorobenzene-d4 9.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 3 3 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 3 4 Formaldehyde O-methyloxime $$ Fo. . . 59 C2H5NO 062479-73-6 2 Abundance Scan 187 (5.509 min): 31638.0 (-) m/z 59.10 100.00% 53

207 5000 43 84 5.20 .N 5.40 5.60 ■ ' I ‘ 5.80 ' I

O-opmpm m/z 207.00 55.41% miz-> 10 2030405060 70 8090100110120130140150160170180190200210 Abundance #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine ... 59

5000 42 TFr 1 1 1 1 • ■ i • ' ■ • i ■ ■ ■ ■ i 5.20 5.40 5.60 5.80 m/z 43.20 32.78%

niz-> 0- TrTTTp-rTTp-rTT]- TTpT ... .|... .|.... | ... . 1 ... . j l|H Abundance

5000 10 2030405060 70 8090 100110120130140150160170180190200210 23 58 #500: 2-METHYL-3,3-D2-AZIRIDINE .<!.. ..{.. ..|.... |....|...

i “i । > j

m/z 5.20 .1 । i .Tl“) ’ ’I***’I 5.40 41.10 5.60 5.80 32.14%

42 O- "i"1 niz-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #648:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine ... 30 5.20 5.40 5.60 5.80 m/z 40.00 16.77% 5000 AoAonpoonow 15 5 44 0 TIITonnr ' 1 1 ‘ ‘ ’ I ‘ ‘ ‘ ‘ I ' ‘ ‘ ‘ I ‘ ‘ ‘ I m/z-> 10 2030405060 70 8090 100110120130140150160170180190200210 5.20 5.40 5.60 5.80

31638.D SCAN508.M Tue Jan 22 08:37:02 2002 Page 5

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