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GCMS analysis results for sample AD31677, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050334–000050348

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050344
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31677.D Vial: 2 Acq On : 23 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.22 ug/L 74483 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 78 2 PROPYLENE GLYCOL TRIMER 1 174 C9H1803 000000-00-0 43 3 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 4 3-Hexanol 102 C6H140 000623-37-0 9 Abundance Scan 567 (9.847 min): 31677.D (-) m/z 59.10 100.00% 59

5000

45 ■ ■. T IM—aayRum |..... 73............. 104............... 9.60 9.80 10.00 10.20

miz-> 01 20 ... 401.5. 30 50 60 70 80 90 100 110 120 130 m/z 45.10 12.73% Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$1-(2-Methoxyp... 59

5000

m/z 9.60 LM 73.10 9.80 10.00 10.20 10.61% 31 45 73 .jnx 0------ T1— J muguB 11* —TTTT130 mz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOLTRIMER 1 50 9.60 9.80 10.00 10.20 5000 41 m/z 58.10 8.69% 103

..................... ...... . ... . 117 130 0- ' i ■ ■ ■ ■ i ■ ■ 1 ■ ■ i ‘ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9600:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 50 9.60 9.80 10.00 10.20 m/z42.10 8.01% 5000 31 73

/z—> 44 0—TT -HH 4—74 1 ■ i ■ ■ ■11 ■ ■ ■ ■ 102 20 30 40 50 60 i 1 ■ ■ • i ■ 1 ■ 1 i ■ 1 ■ ■ i ■ ■ 70 80 90 100 110 120 130 AA.... 9.60 9.80 10.00 10.20

31677.D SCAN508.M Thu Jan 24 09:57:38 2002 Page 7

NYC-WTC_000050344

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NYC-WTC_000050344Source: NYC Law Department, mirrored locally

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