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GCMS analysis results for sample AE10209, May 2002

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Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024333–000024344

Folder label: “GCMS X 5/1/02 A 5/9/02

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NYC 9/11 Public Portal Document

■Data File C:\MSDCHEM\1\DATA\020509\10209.D Vial: 11 Acq On 9 May 2002 8:30 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.37 ug/1 46424 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Vr-phenexthrene - dl 0 188 C14D10 001517-22-2 83 C 2 Antht acene-d10. 188 C14D10 001719-06-8 80 3Pentacyclo [7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 59 4 Selenide, ethyl 1-methyl-1-pente..■ 188 C8H12Se 025128-48-7 38 Abundance Scan 4915 (31.958 min): 10209.D (-4906) (-) m/z 188.15 100.00% 188

5000

43 66 80 94 160 31.60 31.80 32.00 32.20 TLmTIWTTT4— il I 52 ITIWTTTTTmPTTTTT 11, 135 ,1 TTTnr m/z 189.15 20.84% mlz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80 94 160 m/z 184.10 14.54% 30 42 52 66 mz-> TTTTTTTTTTTTTTTTTTTHTTHT .. . 118..132.146/....... . 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance। #79826: Anthracene-d 10- 1t8

31.60 31.80 32.00 32.20 5000 13.49%

RR 80 94 160 17 30 42 52 1|11"I 1 “ 1 I*11 1I1 1"I ° . 1 1 I 1 1 । 1 I 11 1 ' I 11 1 1 I J 108118 132 146 II 1 1 | I ' I I | I । > I |'I I I I | I I ! I | I I I I | I I I’’ I 170179/.. | iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715:Pentacyclof7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... '~rl 1 1 1 ' i 1 ' 1 1 1 1 US 31,60 31.80 32.00 32.20 m/ z 66.20 11.51% 5000 79 91 55 67 0E 117 1 31 410

m/z-> 4 ■ i “ " r ■ ‘11" " i' - 145158173.. 1 L . । /. spiv — -I । । । 11 । । 11 । 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10209.D SCAN020507.M Tue May 14 14:23:02 2002 Page 7

NYC-WTC_000024343

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NYC-WTC_000024343Source: NYC Law Department, mirrored locally

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