NYC 9/11 Public Portal Document
'Data File C:\MSDCHEM\1\DATA\020509\10210.D Vial: 12
Acq On 9 May 2002 9:29 pm Operator: Nefliu
Sample sample Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator)
Title : Method 508 GC/MS Scan
Library : C:\DATABASE\nist98.1
Peak Number 4 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
31.09 0.32 ug/1 40230 Phenanthrene-dl0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 50
2 Bitoscanate 192 C8H4N2S2 004044-65-9 47
3 Bitoscanate 192 C8H4N2S2 004044-65-9 47
4 Pyrdzine, tetraethyl- 192 C12H20N2 038325-19-8 40
Abundance Scan 4768 (31.094 min): 10210.D (-4754) (-) m/z 192.10 100.00%
192
5000
P9 96 146
160 30.80 31.00 31.20 31.40
42 _ 66 1 108 122 " " I1'1" I " 1' I " " I Amp
.. .................. 1 n 11 , ।. ,1, ।, |'k I. । ir TT m/Z 191.10 25.68%
miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid
192
5000
I ........ ,..1.
30.80 31.00 31.20 31.40
89 175 rn/z 146.10 20.00%
— 63 117 145
............. J. .-iip.'..
45 | |
105 11’
.'.A +1TTTTt] HT ‘133
77
135 | 163
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #80930: Bitoscanate
192
30.80 31.00 31.20 31.40
5000 m/z 96.00 18.76%
134
90 160
63 75
n/z->
+26, 394 1 107116
- Ttprri 148
I I I |'I I I 1 | I1!1! TPTTT
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
1 ■ i ■" 11" " i
|................
Abundance #125828: Bitoscanate
1il i 1 1 1 । i । ' ‘ I ‘ ' 1 ' I ' 1
192 30.80 31.00 31.20 31.40
m/ Z 82.10 15.27%
5000
134
90 160
. ..................
50 63 75
I1?2, 122 . 148
++H TTh . TTTH
176
..... ji.... M,,
n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40
10210.D SCAN020507.M Tue May 14 14:23:20 2002 Page 6
NYC-WTC_000024354
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