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GCMS chain of custody form, sample AE10210, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024345–000024356

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024354
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NYC 9/11 Public Portal Document

'Data File C:\MSDCHEM\1\DATA\020509\10210.D Vial: 12 Acq On 9 May 2002 9:29 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 40230 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 50 2 Bitoscanate 192 C8H4N2S2 004044-65-9 47 3 Bitoscanate 192 C8H4N2S2 004044-65-9 47 4 Pyrdzine, tetraethyl- 192 C12H20N2 038325-19-8 40 Abundance Scan 4768 (31.094 min): 10210.D (-4754) (-) m/z 192.10 100.00% 192

5000

P9 96 146 160 30.80 31.00 31.20 31.40 42 _ 66 1 108 122 " " I1'1" I " 1' I " " I Amp .. .................. 1 n 11 , ।. ,1, ।, |'k I. । ir TT m/Z 191.10 25.68% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 I ........ ,..1. 30.80 31.00 31.20 31.40 89 175 rn/z 146.10 20.00% — 63 117 145 ............. J. .-iip.'.. 45 | | 105 11’ .'.A +1TTTTt] HT ‘133 77 135 | 163 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80930: Bitoscanate 192

30.80 31.00 31.20 31.40 5000 m/z 96.00 18.76% 134 90 160 63 75

n/z-> +26, 394 1 107116 - Ttprri 148 I I I |'I I I 1 | I1!1! TPTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 ■ i ■" 11" " i |................ Abundance #125828: Bitoscanate 1il i 1 1 1 । i । ' ‘ I ‘ ' 1 ' I ' 1 192 30.80 31.00 31.20 31.40 m/ Z 82.10 15.27% 5000 134 90 160 . .................. 50 63 75 I1?2, 122 . 148 ++H TTh . TTTH 176 ..... ji.... M,, n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 30.80 31.00 31.20 31.40

10210.D SCAN020507.M Tue May 14 14:23:20 2002 Page 6

NYC-WTC_000024354

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NYC-WTC_000024354Source: NYC Law Department, mirrored locally

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