Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.
NYC-WTC_000044227–000044238Folder label: “GCMS X 4/26/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
'Data File C:\MSDCHEM\1\DATA\020507\10067.D Vial: 27 Acq On 8 May 2002 1:44 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 4 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.32 ug/1 41503 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 64 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 3 Bitoscanate 192 C8H4N2S2 004044-65-9 47 4 Bitoscanate 192 C8H4N2S2 004044-65-9 47 Abundance 1 Scan 4767 (31.088 min): 10O67.D (-4757) (-) m/z 192.10 100.00% 192
5000 h 40 51 64 82 96 119 146 160 30.80 31.00 31.20 31.40 ' ’ I •.. > | . 1 I 1 | u I I | I I I 1 | I I " I'1 1 I 111111 f rd I |‘l 1 I I | 1 I I'l | 1 ri I | I " I1! | I , 11,1, , | | I ll | " 111‘" I I | I iti'i - m/Z 191.00 20.00% m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192
5000 । ■ r ■ ■ । ■ 30.80 31.00 31.20 31.40 175 m/z 146.10 12.05%
„. 63 89 117 145 mmm--4 mm 45 | 77 , 105 , । 135 I 163 rtr > ! I | I'l'l I | l i'l'l |‘l I I I | CI I I | I l'l ! | I , I > |' 4 m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80950:1,5-Naphthalenedithiole 192 ' ■ i ■ ■ 30.80 31.00 31.20 31.40 5000 m/z 193.10 11.69% 115 128 159 40 57 69 79 96 147
m/z-> mPr 111111111111 i‘t । i‘|‘i‘Iii । p i1!1! । r i rerrptemr iJI 11 ii 111 l |' 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 -H . .............. Abundance #125827: Bitoscanate .......... 1 H......... ‘ I ' "id." I "‘I ‘ /‘I’* 192 30.80 31.00 31.20 31.40 m/z 147.30 8.63% 5000 134 50 63 75 90 160
n/z-> 4 ,.14...281.3%m 4l+4,++ 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 148 .... ! ITTT d+ranyannil 30.80 31.00 31.20 31.40
10067.D SCAN020507.M Tue May 14 08:47:27 2002 Page 6
NYC-WTC_000044236
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000044215
Laboratory report documenting GCMS analysis of sample AE10066 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044166
Laboratory report documenting GCMS analysis of sample AE10023 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044203
Laboratory report documenting GCMS analysis of sample AE10061 conducted on May 14, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044132
Laboratory report documenting GCMS analysis of sample AE10020 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044191
Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045707
Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044156
Laboratory report documenting GCMS analysis of sample AE10022 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044179
Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044144
Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044119
Laboratory report documenting GCMS analysis of sample AE10019 conducted on May 14, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024345
Chain of custody record for GCMS analysis of sample AE10210 on May 20, 2002, including surrogate compound data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024333
Laboratory report detailing GCMS analysis of sample AE10209 conducted on May 20, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044098
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 26 and May 8, 2002.
Filed in the same folder
NYC-WTC_000044099
Fragmented page from a GCMS record series dated between late April and early May 2002 regarding environmental sampling analysis.
Filed in the same folder
NYC-WTC_000044100
Laboratory blank report for sample AE10019 showing non-detectable levels of target compounds from May 7, 2002.
Filed in the same folder
NYC-WTC_000044107
Laboratory report showing blank analysis results for sample AE10019 conducted between April and May 2002 with no detected contaminants.
Filed in the same folder
NYC-WTC_000044111
Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.
Filed in the same folder