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GCMS analysis results for sample AE10208, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10208 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024319–000024332

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024326
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.32 ug/1 50112 Phenanthrene-dl0 31.72

Hit# of Tentative ID MW MolForm CAS# Qual

1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 53 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 46 4 Bitoscanate 192 C8H4N2S2 004044-65-9 43 Abundance Scan 4767 (31.088 min): 10208.D (-4756) (-) m/z 192.10 100.00% 192

5000 82 1111** 146 ..... 49 66 118 1 164 |221 326 -rp-T 11‘111111111"1111111101111113711"T 30.80 31.00 31.20 31.40 m/z 82.10 23.24% nz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamicacid 192

5000 AAL 30.80 31.00 31.20 31.40 175 m/z 191.20 22.94% 45 3 89 117 145 Hri , A A P . 4 .. 11 ■ ■ ■ ■ i'■1'।■1■r।■1'' । ■■1 ■ i' ■ ■ ■ i ■ ■ n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #125845: Anthracene, 2-methyl- 192

30.80 31.00 31.20 31.40 5000 m/z 193.10 15.75%

96 165

m/z-> 0 75 । 115 139 TRTTTTT IT’II’IU’BII311AA’’’’IUEAUIII’’I’ | , 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 4 Abundance #80862:1,2-Phenylene diisothiocyanate 102 30.80 31.00 31.20 31.40 m/z 146.20 14.60% 64 5000

90 134 39 , 160 a0814k444444+++. TTTT ' i " ' ■ i ■ " 1 r ''' i ■ " ' i ■ " ' i1" ' i' ■ k............... ■ ■ i 1 ' 1 ' i * I ' 1 ' ' 1 1 1 n/z—> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.80 31.00 31.20 31.40

10208.D SCAN020507.M Tue May 14 14:22:32 2002 Page 4

NYC-WTC_000024326

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NYC-WTC_000024326Source: NYC Law Department, mirrored locally

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