GCMS analysis results for sample AE10024, May 2002

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Laboratory report documenting GCMS analysis of sample AE10024 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044179–000044190

Folder label: “GCMS X 4/26/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020507\10024.D Vial: 23 Acq On 8 May 2002 9:48 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************* * * * ****** * * * Peak Number 4 3,4-Methylenedioxycinnamic ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.31 ug/1 34552 Phenanthrene-dl0 31.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Methylenedioxycinnamic acid 192 C1OH804 002373-80-0 59 2 Anthracene, 1-methyl- 192 C15H12 000610-48-0 53 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 4 Phenanthrene, 2-methyl-_____________ 192 C15H12 002531-84-2 53 Abundance 7 Scan 4769 (31.100 min): 10O24.D (-4756) (-) m/z 192.20 100.00% 192

5000 96 49 70 82 146 | 164 30.80 31.00 31.20 31.40

/z-> । ■ ■ ' ■ । 1 0 20 , , , ,111,1111, । , J, 1,14-1-’I | 1 1 1 1 | 40 60 80 '100 120 120 ■ 1 ( > *'11 I | I , . , , . . 140 160 180 200 m/z 191.10 43.63% Abundance #81021: 3,4-Methylenedioxycinnamic acid 192

................. i «............ A 5000 111' ■1111 ■111'111111 30.80 31.00 31.20 31.40 63 89 145 175 m/z 96.00 25.80% 11 4 14 29 39 51 1, 77 117 135 li, ,.,1^,4,,. I. .. II '■'I1"'-' 1* ■1 r ■ ' 11 । 11 ■' ' 163 105 (li l ■ m/z->0 20 40 I60 80 100 120 140 160 180 200 Abundance #125853: Anthracene, 1-methyl- 192

30.80 31.00 31.20 31.40 5000 m/z 146.10 15.05% 165 44 63 74 86 96 115126 139 152 . 176 —। । । । । । i । । । । I-1 "i । । ‘'i i-1 "r r4ll lerr । ।-i—। 1 1 1 " । rli - m/z-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #125846: Anthracene, 2-methyl- 192 A ' ' I ' ' r ' i 1 30.80 31.00 31.20 31.40 m/z 49.05 13.50%

5000

165 4 15 27 39 51 63 83 9 ■n/z-> 0 1**III1**1**1*I0I1/mdm 20 40 60 80 100 115126 139 152 1 ■ i ■ ■ ■ 1 i ■ 120 140 TF 160 L 176 I 180 200 1 I ' ' 30.80 31.00 31.20 31.40

10024 .D SCAN020507.M Tue May 14 08:45:58 2002 Page 6

NYC-WTC_000044188

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GCMS analysis results for sample AE10021, May 2002 · Box DEP Box 25

NYC-WTC_000044144

Laboratory report documenting GCMS analysis of sample AE10021 conducted on May 14, 2002, identifying unknown compounds.

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