GCMS sample analysis results for AE10698, May 20 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Bitoscanate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.29 ug/1 28560 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 43 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 40 3 Bitoscanate 192 C8H4N2S2 004044-65-9 37 4 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 37 Abundance Scan 4768 (31.094 min): 10698. D (-4757) (-) m/z 192.10 100.00% 192

5000

96 146 1 । | i r~T i | । । 1s P 11 1 । i 42 66 h ill itAn II 1 । । । r > । । । i r | L....... 217........... 444 1. 1 1 30.80 31.00 31.20 31.40 m/z 191.10 29.51% •n/z-> 50 100 150 200 250 300 350 400 450 Abundance #125828: Bitoscanate 192

5000 I 30.80 31.00 31.20 31.40 134 m/z 146.10 20.58% c 90 160 ।

n/z-> 4QlL 50 100 150 200 250 ‘1*1**++‘‘I‘‘1IIII 300 350 400 450 Abundance #80950:1,5-Naphthalenedithiole 192 .......II....... 30.80 31.00 31.20 31.40 5000 m/z 96.20 19.68% 128 159

mfe-> —1 44,1 40

50 79 1 02

100 150 200 250 ' I 300 ' ' 1 ' I 1 ' ' ' 350 | > 1 1l 400 l r-T r—k 450 Abundance #80930: Bitoscanate 192 30.80 31.00 31.20 31.40 m/z 193.20 18.44% 5000 134 160 , 63 90

m/z-> ,3144441 50 100 150 1 1 200 ' 1 ’ ' 250 1 1 ' ‘ 1 1 300 1 ' ' 1 350 I 1 1 1 400 1 1 1 1 1 T" 450 .............. 1 1 L 30.80 31.00 31.20 31.40

10698.D SCAN020507.M Wed May 15 08:33:46 2002 Page 7

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