GCMS results for sample AE11426, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11426.D Vial: 12 Acq On : 21 May 2002 7:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Bitoscanate Concentration Rank 3 R.T. EstCono Area Relative to ISTD R.T. 31.09 0.27 ug/1 29829 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Bito scanate 192 C8H4N2S2 004044-65-9 38 2 Thiazole, 2-(phenylthio)- 193 C9H7NS2 033342-67-5 37 3 Bito scanate 192 C8H4N2S2 004044-65-9 37 4 Cyclphexanamine, N-cyclodecylidene-235 C16H29N 074810-29-0 33 Abundance Scan 4767 (31.088 min): 11426.D (-4758) (-) m/z 192.10 100.00% 192

5000 96 146 1 ■ i ■ ' ' ' i ‘ I’’

m/z-> 43 70 0— 1 1 l,i il ,1 0 ■ ■ 1 i

50 ■ ' ■ ■

100 i ’ ■ L 150 200 )T , , 250 502 .................. .......................................... 1 , 300 350 400 450 500 30.80 31.00 31.20 31.40 m/z 191.10 26.19% Abundance #125827: Bitoscanate 192

5000 A.M1....... 134 30.80 31.00 31.20 31.40 50 90 160 m/z 96.00 21.71%

0 27alll1. n/z-> 0 50 100 150 200 250 300 . 350 400 450 500 Abundance #81050: Thiazole, 2-(phenylthio)- 192 ill I.... f' I ‘ II" 30.80 31.00 31.20 31.40 5000 m/z 193.20 20.91%

58 109 148 [ O—I ,, mz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #80930: Bitoscanate 192 30.80 31.00 31.20 31.40 m/z 146.20 19.10%

5000 134 160 63 90

n/z-> 0 —4 0 50 100 150 200 250 300 350 400 450 500 1 ' I ' ' ' ' I ' ' I ' ' • ■ I ' I 30.80 31.00 31.20 31.40

11426.D SCAN020521.M Fri May 24 09:28:42 2002 Page 5

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