GCMS analysis results for sample AE10301, May 10, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020509\10301.D Vial: 26 Acq On : 10 May 2002 11:20 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Bitoscanate Concentration Rank 3 R.T. EstConc Area Relative to. I STD R.T. 31.08 0.34 ug/1 44607 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Bitoscanate 192 C8H4N2S2 004044-65-9 50 2 Pyrazole, 3-(p-chlorophenyl)-5-m... 192 C10H9C1N2 017629-27-5 42 3 5H-Dibenzo [a, d] cycloheptene 192 C15H12 000256-81-5 42 4 Phenanthrene, 4-methyl-_____________ 192 C15H12 000832-64-4 38 Abundance ' Scan 4765 (31.076 min): 10301 .D (-4754) (-) m/z 192.10 100.00% 192

5000

146 36 ,70.84 1207s 441 ■ ■ i 30.80 31.00 31.20 31.40 m/z 193.00 18.67% m/z-> 50 100 150 200 250 300 350 400 Abundance #125828: Bitoscanate 192

5000- * ' I ' ' v 1 I ' ' 30.80 31.00 31.20 31.40 134 m/z 146.20 13.66% 63 90 160 ,494 44h,al1a / 1, n/z-> 50 100 150 200 250 300 350 400 ft Abundance #81077: Pyrazole, 3-(p-chlorophenyl)-5-methyl- 192

30.80 31.00 31.20 31.40 5000 m/z 191.00 12.53% 42 75 128

15 41 . J k 101 1 151 ---------- | n/z-> 50 100 150 200 250 300 350 400 Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192 / NAM.. 30.80 31.00 31.20 31.40 m/z 160.20 11.67%

5000

89 165 39 63 111,115 139,1, + —T11 ri111’ r11 m/z--> 50 100 150 200 250 300 350 400 30.80 31.00 31.20 31.40

10301.D SCAN020507.M Tue May 14 14:26:54 2002 Page 4

NYC-WTC_000024932