GCMS analysis results for sample AE11154, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11154.D Vial: 19 Acq On : 22 May 2002 2:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Bitoscanate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.23 ug/1 24160 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 32 2 4-Nitrobenzoylacetone 207 C10H9NO4 1000130-56-3 32 3 Bitoscanate 192 C8H4N2S2 004044-65-9 32 4 5- [5-iyiethylfurfurylidene] hydantoin 192 C9H8N2O3 1000214-69-2 17 Abundance Scan 4768 (31.094 min): 11154.D (-4760) (-) m/z 192.20 100.00% 1512

5000

82 96

m/z—> 01 20 40 43 60 66 80 100 . 122.. 1s 1s0 120 140 160 180 242 i ' i ' ' ' 1 i ■ ' 1 ' i ■ ' 200 220 240 ■ > । ■ > ■ ■ । ■ 30.80 31.00 31.20 31.40 m/ Z 193.20 T4TT 24.16% Abundance #125828: Bitoscanate 192

5000 „I... 1 30.80 31.00 31.20 31.40 134 m/ z 82.10 21.73% 50 63 75 90 102 1 160 148 176 I...... ............ O+ -------- 1 11 ■ 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #81094: 4-Nitrobenzoylacetone 192 1........ ....... I ' I ‘ ' 1 I ‘‘ 30.80 31.00 31.20 31.40 207 5000 m/z 95.90 21.53% 43 69 85 146 160 105 0 i ' 1 1 ' r ■ 1155 I -1“1. 4— ,120131 । I , . I TTIl Tu 1 176 ' 1 i ' 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #80930: Bitoscanate 192 30.80 31.00 31.20 31.40 m/z 146.10 15.77%

5000 134 on 160 4 50 63 75 I 107

m/z-> 0 —26.394—1——L44L41I4 frir 122 '''* i r ■ , -r 148 l ...................... 11 i 11■1 r1 1 1 1 i 1 1 1 ' i ' • ■ 1 i '■ ■ i ■ ■ ■ ■ i ' ' 20 40 60 80 100 120 140 160 180 200 220 240 30.80 31.00 31.20 31.40

11154.D SCAN020521.M Fri May 24 09:23:30 2002 Page 8

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