Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
NYC-WTC_000025542–000025555Folder label: “GCMS X 5/17/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11154.D Vial: 19 Acq On : 22 May 2002 2:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 2-Propen-1-one, 3-(4-chloro... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.23 ug/1 23896 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propen/1-one, 3- (4-chloropheny. . . 242 C15H11C1O 000956-04-7 12 2 2-Bromo-4,6-difluoroaniline 207 C6H4BrF2N 000444-14-4 12 3 Quinoline, 3-bromo- 207 C9H6BrN 005332-24-1 12 4 Quinoline, 3-bromo-______________ 2 07 C9H6BrN 005332-24-1 12 Abundance 7 Scan 4394 (28,896 min): 11154. D (-4386) (-) m/z 209.10 100.00% 2(19
242 5000 49 61 84 101 137 39 120 167 L 11 ■ ■ rb ■ * 1 i * ■ * * । 28.60 28.80 29.00 29.20 0 । 1 * ■ ■ । ■ 1 ■ ■ । > 1I m/ Z 207.00 74.32% miz- > 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #91631: 2-Propen-1-one, 3-(4-chlorophenyl)-1-phenyl- 242
5000 77 105 165 207 A28.60 28.80 29.00 29.20 51 89 137 179 m/z 241.90 61.29% XI 1. .4. I1 ,1 'I,l ... . 225 A 0 i ■ ■ 1 ' I 1 ■ 1 1 i 1 ■ ‘ i ■ 11 1 1 I 1 1 11 1 1 1 1 1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #85327:2-Bromo-4,6-difluoroaniline 209 ' ' I ' ' ' ■ I ' 1 ' ‘ I ' ‘ ' 1 1 ' I 28.60 28.80 29.00 29.20 5000 108 128 m/z 244.00 61.03%
81 31 52 64 179 0!— —lL—+lu allL 1 ■ i ' ' ' • i 1 ' m/z-> Abundance 20 40 60 80 100 120 140 160 180 #126483: Quinoline, 3-bromo- 128 200
207 220 240 ....... .. .....I, 28,60 28.80 29.00 29.20 m/z 101.00 42.06% 5000 101 75 50 64 90 0 TIr ||I -ll , 117 141 155 181 ■ i ■ • ■ ■ i ■ * m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20
11154.D SCAN020521.M Fri May 24 09:23:29 2002 Page 7
NYC-WTC_000025552
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NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022526
Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024390
Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046147
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045778
Gas chromatography-mass spectrometry report for sample AE10703 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Laboratory log sheet recording Method 608 extraction parameters and sample counts for sample AE11423 in May 2002.
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Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
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Laboratory report of GCMS reference standard analysis showing response values for 15 volatile organic compounds on May 17-21, 2002.
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