GCMS analysis results for sample AE08970, May 7, 2002

NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\l\DATA\020424\08970.D Vial: 18 Acq On : 25 Apr 2002 2:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Bitoscanate Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.35 ug/1 652091 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bitoscanate 192 C8H4N2S2 004044-65-9 59 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 45 3 5H-Dibenzo(a,d]cycloheptene 192 C15H12 000256-81-5 45 4 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 Abundance Scan 4768 (31.094 min): 08970.D (-4755) (-) m/z 192.10 100.00% 192

5000 ................ ....... .................... 40 82 146 । 30.80 31.00 31.20 31.40 11 ■ -5 I J 118 h ■' ri"i m/z 40.10 29.72% ■n/z-> 50 100 150 200 250 300 350 400 450 500 RWWWAMAwWMWWwMWwtW

Abundance #125828: Bitoscanate 192

5000 1 1 1 I ‘ ' ‘ I ' ' 1 r r i" 30.80 31.00 31.20 31.40 134 160 m/z 191.10 18.45% 63 90 4944), miz-> 50 100 150 200250300350400450500 Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 192 163 30.80 31.00 31.20 31.40 5000 m/z 82.10 14.07% 68

miz-> -A21 50 100 150 200/250 300/350 400 450 500 Abundance #80999:5H-Dibenzo[a,d]cycloheptene 192 30.80 31.00 31.20 31.40 m/z 193.00 13.94% 5000

165 89 , 38,6344115139., 4,__ _________ 1 1 i 1 ■ z—> 50 100 150 200 250 300 350 400 450 500 30.80 31.00 31.20 31.40

08970.D SCAN020424.M Thu May 02 15:01:24 2002 Page 7

NYC-WTC_000049668