GCMS analysis results for sample AE08970, May 7, 2002

NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\020424\08970.D Vial: 18 Acq On : 25 Apr 2002 2:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 1-Butanamine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.27 1.07 ug/1 1285580 1,4-Dichlorobenzene-d4 11.38 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1-Butanamine 73 C4H11N 000109-73-9 4 2 1-Butanamine 73 C4H11N 000109-73-9 4 3 1-Hydroxy-2-butanone 88 C4H802 005077-67-8 4 4 1-Hydroxy-2-butanone 88 C4H802 005077-67-8 3 Abundance Scan 544 (6.276 min): 08970.D (-542) (-) m/z 40.10 100.00% • 40

5000-

xd/nnn/mB—BBmBBTmgann 49 50 69 73 88 6.00 6.20 6.40 6.60 miz-> Abundance o 5 10 15 20 25 30 35 40tmmptpmkpm .। ।।.... 45 50 55 60 65 70 75 80 85 90 95 #108242:1-Butanamine m/z 49.05 8.90%

30

5000 1 ■ ■ ■ । * • • • । ■1 ■ । ■r 11111' 6.00 6.20 6.40 6.60 m/z 48.00 5.60% 73 , 37,4.45 51 56 60 68 | m/z-> Abundance o . 5...................... Tamgomnp—enmpggm 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #108149:1-Butanamine 30 6.00 6.20 6.40 6.60 5000 m/z 69.10 5.16%

, 37,41.45 50 56 60 64 68 73 2 .... . ............. ... HpHmmgu miz—> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #477:1-Hydroxy-2-butanone ,‘ • * 1) ’ k ........ 8t I 18s 1*** 29 6.00> 6.20 6.40 6.60 57 m/z 50.30 4.79% 5000

iz—> 33 38 42 49 53, 15 20 25 HTH Tpm 0 6973 510 15 20253035404550 556065 70 75 80859095 88 । AMLJNAALl 6.20 6.40 6.60 ‘ 6.00

08970.D SCAN020424.M Thu May 02 15:01:22 2002 Page 6

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