GCMS analysis results for sample AE10023, May 2002

NYC 9/11 Public Portal Document

' Data File C:\MSDCHEM\l\DATA\020507\10023.D Vial: 22 Acq On 8 May 2002 8:49 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Pentane, 2-nitro Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.01 2.32 ug/1 194078 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 2-nitro 117 C5H11NO2 1000196-88-0 53 /2 Butenol, methyl- 86 C5H10O 060766-00-9 50 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 47 4 Propanoic acid, 2-methyl-, anhyd... 158 C8H14O3 000097-72-3 43 Abundance Scan 328 (5.006 min): 10023.D (-322) (-) m/ z 43.10 100.00% 43 71 5000 55 “I । । i । i । rn-1 । । । । । । ' । i i i~r । । ।

m/z-> ' ‘ 1 1 ' 1 ' T 1 20 40 1 i 80 60 87 97 221 ............... I 1 * 1 ■ i 1 1 1 1 । 100 120 140 160 180 200 220 * 1 1 । । 1 1 |-i । 4.60 4.80 5.00 m/z 41.10 5.20 5.40 68.82% Abundance #6270: Pentane, 2-nitro 43

5000 71 ATn rmmor Arm" 29 4.60 4.80 5.00 5.20 5.40 55 m/z 71.10 67.44%

J_ TT 87 100 118 11 I*/*/*II‘‘‘IIIIFU*IIIIIII‘IIIIIIIII T' 1 m/z-> 20 40• 60 80 100 120 140 160 180 200 220 Abundance #24435: Butenol, methyl- 43 71 fTTr 4.60 4.80 5.00 5.20 5.40 5000 59 m/ Z 69.20 58.82% 27 15

‘ 'I 1 "A- al4ill— 186 m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #24438: 3-Buten-2-ol, 2-methyl- ' i ' ' ‘rId—m—RR—TtTT 71 4.60 4.80 5.00 5.20 5.40 m/z 55.05 32.58% 43 5000 59 27 151 1 I II111 11 I—1 .86................. 1 ■ i ■ ' 1 ■ । 1 1 • ■ i > ■ > ■ ) ■ > ■ ■ i • ■ ■ ■ । > । ■ । I 1 1 1 । I । 1 4 i, n/z-> 20 40' 60 80 100 120 140 160 180 200 220 4.60 4.80 5.00 5.20 5.40

10023.D SCAN020507.M Tue May 14 08:45:36 2002 Page 3

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