GCMS analysis results for sample AE10024, May 2002

NYC 9/11 Public Portal Document

Data File C : \MSDCHEM\1\DATA\020507\ 10024 .D Vial: 23 Acq On 8 May 2002 9:48 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Pentane, 2-bromo- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.01 2.37 ug/1 188615 1,4-Dichlorobenzene-d4 11.38

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 2-bromo- 150 CSHllBr 000107-81-3 50 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 3 Butanol, methyl- 86 C5H10O 060766-00-9 50 4 Tetrahydrofurfuryl acrylate 156 C8H12O3 002399-48-6 47 Abundance Scan 328 (5.006 min): 10024.D (-323) (-) m/ z 43.05 100.00% 43 , 71

5000

4.60 4.80 5.00 5.20 5.40 Jni.................... 207.............................................................. 541 m/z 41.10 83.07% i ' 1 m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #109867: Pentane, 2-bromo- 43 71

5000 A-PyTrmm 4.60 4.80 5.00 5.20 5.40 m/ z 71.10 78.46% 18 107 150 i ' ' FT—dmD///mETdmBmmU-T Ti/Z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #114555: 3-Buten-2-ol, 2-methyl- 43 71 ‘I’sI’II* ‘rn rr Y ' I ' t 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 63.83%

11*14 1 1 1 m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #24435: Butenol, methyl- ----------- 43 71 4.60 4.80 5.00 5.20 5.40 m/ z 55.10 37.11% 5000

/z—> 100 150 200 250 300 350 400 450 500 4.60 4.80 5.00 5.20 5.40

10024.D SCAN020507.M Tue May 14 08:45:51 2002 Page 3

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