GCMS analysis results for sample AE08970, May 7, 2002

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Laboratory report documenting GCMS analysis of sample AE08970 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049658–000049670

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\020424\08970.D Vial: 18 Acq On : 25 Apr 2002 2:34 am Operator: Nefliu Sanpl e : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.29 ug/1 526355 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 86 2 Nickel, di-.mu.-carbonylbis(.eta... 302 C12H10Ni2O2 012170-92-2 43 3 4-[4-Acetamido-l-pentylamino]-1-... 302 C16H22N4O2 1000213-35-9 33 4 Phenant hrene-dl0 188 C14D10 001517-22-2 32 Abundance Scan 4915 (31.958 min): 08970.D (-4908) (-) m/z 1 88.10 100.00% 188

5000

40 94 ’E I ' • ‘ 1 I ‘ ‘ ' I ' ' ‘ I ‘

11 I t. 66 .1 ’ • ii.,, jr,. " i ' 1 1 ■ i ' ■ ■ ■ i ■ ' ■ ■ i 368 ■ ‘ ■ i ■ ■ ■ • I ■ ‘ 492 i 31.60 31.80 32.00 32.20 m/z 189.20 21.10% miz-> 50 100 150 200 250 300 350 400 450 Abundance #79826: Anthracene-d10- 188

5000 F ------- 31.60 31.80 32.00 32.20 m/z 40.10 17.44% . 54 160 17 42.66, 1.132 4 . J • ' 1 ‘ 1 1 ‘ ‘ 1 r • r d/nt « 1 । ■ ■ ■ ■ i ■ ■ ■ ‘ । 1 1 ■ ■ । ■ ■ • ■ i ■ 1 1 ■ । 1 T miz-> 50 100 150 :200 250 300 350 400 450 Abundance #79885: Nickel, di-.mu.-carbonylbis(.eta.5-2,4-cyclopentad... 188 1 l 1 1 1 ■ i ■ ■ • • i • • 1 ■ i ■ ' 1 1 i 246 31.60 31.80 32.00 32.20 5000 123 m/z 184.10 17.24%

28 58 97

miz-> 14k 50 .. 4. 100 1 ,154 1 ,218 ... ----- 150 200 250 274327 300 350 ......... 1 11 ‘ i • ■ ■ 1 i ■ ' ‘ ‘ i ' • 1 ■ i ■ ■ ■ ‘ i 400 450 Abundance #79818:4-[4-Acetamido-1-pentylamino]-1 -methyl 1,5-naphthy... 188 TF ' 1 ’ r1 *11**IIII4’11 44 31.60 31.80 32.00 32.20 84 243 m/z 94.10 16.03% 5000

। 131 _ 44ky2Zlu. 4,216 . 302 1,4 1269 1 t_____________________________________________ r 1 ■ ■ • i ■ ‘ • i • ■ ■ 1 i ‘ ■ i ------- m/z—> 50 100 150 200 250 300 350 400 450 31.60 31.80 32.00 32.20

08970.D SCAN020424.M Thu May 02 15:01:26 2002 Page 8

NYC-WTC_000049669

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GCMS analysis results for sample AE08964, May 7, 2002 · Box DEP Box 27

NYC-WTC_000049622

Laboratory report documenting GCMS analysis of sample AE08964 conducted on May 7, 2002, by analyst DLV.

1 shared topics · Same agency, volume and box · similarity 0.997