GCMS analysis results, Sample AE08269, April 22, 2002

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GCMS analysis report for sample AE08269 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048436–000048455

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \MSDCHEM\1\DATA\020417\08269.D Vial: 25 Acq On : 18 Apr 2002 5:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.60 ug/L 1086070 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 56 2 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 3 Anthracene-dlO- 188 C14D10 001719-06-8 40 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3420 (23 174 min): 08269.D (-3414) (-) m/z 188.10 100.00% 188

5000

■ I । ■ ' I | 'T- ‘ t I ' ■ । | ' I ' 88 94 160 22.80 23 00 23 20 23.40 23.60 57 66 132 146 । n/z-> 43 0- T l tn p l|-r‘|,i । 11‘| l l'i I fl 11 । 11 11 i 111 11 | rm 11 ri 11 rrb pdhoouspov 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 44 m/z 189.10 17.84% Abundance #79827. Phenanthrene-d10 108

5000 _ ----- 22 80 23.00 23 20 23.40 23 60 m/z 94.05 17.56% 80 94 30 42 52 66 160 A n/z-> 10 | 102110118 132 146 0 IWTIITTTTTTTH I !■ ■ [ n ■ ■ 1111111 r.»| f n ■ । >vn ;i-r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 17019, — Abundance #79739: Cycloheptanone, 4-phenyH 188 117 - 104 22 80 23 00 23.20 23.40 23.60 91 160 5000 131 m/z 184.10 14.48% 170 27 33 51 65 78 145

n/z-> 0 1111 ii 111 1 । ri im , hi llpark IM — bal.— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 r i" Tr Abundance #79826. Anthracene-d10- 108 22.80 23 00 23 20 23.40 23.60 m/ z 80.05 11.92%

5000

KK 80 94 160

0 17 30 4 2 52 00 | ,1102 118 132 146 (| 170 180 111111i1111111111 n 11II ri 111 rr 111 fr 11 rtf 11111111111111 111111 ri 111111111 rl'fi ।11111111 i'I'I TTr .. s.... n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22 80 23 00 23 20 23.40 23.60

08269.D 041702SCAN.M Thu Apr 18 10:02:31 2002 Page 14

NYC-WTC_000048453

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