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GCMS sample analysis report AE08483, May 7 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

NYC-WTC_000048623–000048634

Folder label: “GCMS X 4/10/02 A 4/20/02

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Scanned page image, NYC-WTC_000048633
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08482.D Vial: 19 Acq On : 20 Apr 2002 1:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 **************************** * * *************************************** Peak Number 5 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.34 ug/1 733203 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 Antipyrine 188 C11H12N2O 000060-80-0 50 4 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 45 Abundance Scan 4914 (31.952 min): 08482.D (-4907) (-) m/z 188.20 100.00% 188

5000 40 80 94 TII ---------------------- 31.60 31.80 32.00 32.20 49 66, ..1 132 146 158 m/z 40.10 18.57% • i • • • > i • • * • i • ■' ■ ’*’ ■ ‘'r ■ TIHp • i ■ ■ ■ ■ i ■ 1’187 m/z-> 10 20 30 40 50 «) 70 80 90 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 m/z .80.00 17.13% 94 80160

n/z-> 30 42 52 66 . TWWWmWPTTTTTTTTt j| 108118 132 146 ■JTTTT 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 +441791791 Abundance #79826: Anthracene-d10- 188 *"T I 1 TTT! > I . . | t . . I | >■ 31.60 31.80 32.00 32.20 5000 m/z 184.20 15.69%

ee 80 94 160 17 30 42 52 V . . 108118 132 146 I. i ■170179 L । .... 111 > TTTtTTT | 11111 111 . ।I 11 1.111 11. | 11 111 p 11111111 |I l ! 111 r 1111 > i | > > ■ i rt’lt mi miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79725: Antipyrine 188 31.60 31.80 32.00 32.20 96 m/z 189.20 15.66%

5000 77 56 105 27 i ■39 TUTpup 38 67 Jl'Pi ■ ■ Ji dpdpnpoh . Il 115 JmhTpmIL ■ I ’ ’* 130 145 159 173 1 ’T f , . r-T-, , . ■, , । ■ , , , । , n/z—> 10 20 30 40 50 60 70 80 90 100 110120130140 150160170180 190 31.60 31.80 32.00 32.20

08482.D SCAN020418.M Thu May 02 11:44:35 2002 Page 7

NYC-WTC_000048633

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NYC-WTC_000048633Source: NYC Law Department, mirrored locally

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