GCMS analysis results for sample AE08323, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 7 p-Terphenyl-dl4 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

39.23 0.20 ug/1 402682 Chrysene-dl2 39.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 p-Terphenyl-dl4 244 C18D14 001718-51-0 59 2 1,4-Cyclohexadiene, 6-methylene-... 244 C19H16 018636-59-4 42 3 1-Pyrenecarboxaldehyde hydrazone 244 C17H12N2 076465-53-7 42 4 4-Pyrimidinol, 2-(1-methylethyl)... 244 C14H16N2O2 1000197-09-0 40 Abundance Scan 6152 (39.226 min): 08323. D (-6146) (-) m/z 244.10 100.00% 24.4

5000 40 122 IT 1 I ' ' ■ ■ 1 1 1 198 212 I 38.80 39.00 39.20 39.40 39.60 1 55 85 107 , --------------- ------- m/Z 243.10 1 ' I ’ 50.04% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92199: p-Terphenyl-d14 244

5000 i ■ ■ ■ ■ i ■ ■ 1 1 I 1 1 1 1 I 1 1 38.80 39.00 39.20 39.40 39.60 m/z 40.10 31.56% _ 122 18 30 42 54 66 80 94 106 | 136 160172184 198 212 226 , TTT——m9—+t ■ ■ 1 1 ■ "OT --4 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92196:1,4-Cyclohexadiene, 6-methylene-3,3-diphenyl- 24.4 i ■ ■ ■ ■ i 38.80 39.00 39.20 39.40 39.60 5000 m/z 122.10 25.23% 167 229 51 63 77 91 115 128 141152 202 215 11 .,1 11 I ' 11 1 I' 1 ' pdu ■ T /z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92197:1-Pyrenecarboxaldehyde hydrazone ... . 2'4 38.80 39.00 39.20 39.40 39.60 m/z 245.10 22.09% 5000 201 228 100 122

/z—> .49 63 84 t । 111 | 135 150 163174 189 , , 11“1/1—1/n/1//0/1/0/0d/mmmTTTTTTTTT ———l 213 ..... JI..... .. 20 40 60 80 100 120 140 160 180 200 220 240 38.80 39.00 39.20 39.40 39.60

08323.D SCAN020418.M Thu May 02 15:23:57 2002 Page 9

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