GCMS analysis results for sample AE08425, May 2002

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Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 10 p-Terphenyl-dl4 Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 39.22 0.38 ug/1 647331 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 p-Terphenyl-dl4 244 C18D14 001718-51-0 64 2 1,4-Cyclohexadiene, 6-methylene-... 244 C19H16 018636-59-4 64 3 4-Pyrimidinol, 2-(1-methylethyl) ... 244 C14H16N2O2 1000197-09-0 59 4 1,1,1-Triphenyl- 2-decanol 386 C28H340 1000197-22-7 59 Abundance Scan 6151 (39.220 min): 08425.D (-6142) (-) m/z 244.10 100.00% 24.4

5000

122 k 1 w i 1 ■ ■ ■ i ' ' 56 41 77 94 107 1 145 170 197 212 38.80 39.00 39.20 39.40 39.60 onjunalda 4- t /1^, ,4 all ........... i, ' ’ I 1 ll' ' ' I ' ‘ ‘I1 m/z 243.10 46.13% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92199: p-Terphenyl-d14 244

5000 .......... 3............. 38.80 39.00 39.20 39.40 39.60 m/z 245.10 23.10% „ 122 18 30 42 54 66 80 94 106 | 136 160172 184 198 212 226 I —IPI++1eTr 1T1' ■'1111 ' '‘i1 '"I"11'1"1 ■ । r1'' /z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92196:1,4-Cyclohexadiene, 6-methylene-3,3-diphenyl- 244

38.80 39.00 39.20 39.40 39.60 5000 m/z 122.00 15.98% 167 229 51 63 77 91 115 i28141 152 202 215 ■ ■ i ‘ ' i ' 1 1 ' i ■ ' ■ ■ l ■ ■ ■ "V‘ I I I I I I I I I I — Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #92101: 4-Pyrimidinol, 2-(1-methylethyl)-6-I(phenoxy)methyl]- 244 38.80 39.00 39.20 39.40 39.60 m/z 242.00 15.36% 5000 70 43 224 158 28 55 । 82 | _ 123 138 108 . 94 _ 11

/z—> - ral । J 20 40 60 80 100 120 140 160 180 211—7 2001 220 240 TtT 38.80 39.00 39.20 39.40 39.60

08425.D SCAN020418.M Thu May 02 15:28:12 2002 Page 12

NYC-WTC_000048163

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