GCMS analysis results for sample AE08425, May 2002

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Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02”

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Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 11 2-Pentanol, 5-(2-propynyloxy)- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 40.30 0.28 ug/1 484484 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, 5-(2-propynyloxy)- 142 C8H14O2 055702-67-5 9 2 3-Hydroxy-2-methylglutaric acid ... 190 C8H14O5 056652-39-2 9 3 2-Buten-l-amine, N-butyl-, (E)- 127 C8H17N 062337-86-4 5 4 1-Tetradecanamine 213 C14H31N 002016-42-4 5 Abundance Scan 6335 (40.301 min): 08425.D (-6326) (-) m/z 40.10 100.00% 43

5000 57 71 85 98 112 127 141 154165 213 40.00 40.20 40.40 40.60 — 1 1 i ' 1 1 1 1 in1 rI 1 1,1 r' 1 ' . 1 I 1 1 .I 1 ,' 1 1 nil 1 ’. H I 1 11li ■ I__ ■ ■ i m/z 57.15 29.47% m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance 39 #1282: 2-Pentanol, 5-(2-propynyloxy)-

wolulupt 5000 29 T r-| ‘ CI 71 40.00 40.20 40.40 40.60 55 85 m/z 71.20 28.68% 15 a— n/z-> Abundance 20 23 40 ll 1 i ' 60

71 85 I, ill. 11 ‘ T 1 80 ' ' 98 112123 i ■'' । 100 #108107: 3-Hydroxy-2-methylglutaric acid dimethyl ester 141 ■ | , । । । | I > 120 140 I ! | I । I । | I । । । | I । 160 180 200 । । |

pp/hutui 103 56 117 40.00 40.20 40.40 40.60 5000 m/z 43.10 20.99% 130 JwphpuralMw/ukwup I 159 ■ ■ । ■ ‘ i ’ ■ i ■ ■ ■ ■ i ■ 1 i 1 ' ■ ' I ■ ' ■ ■ i ■ ' ' ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #806: 2-Buten-1 -amine, N-butyl-, (E)- 33 40.00 40.20 40.40 40.60 m/ z 85.10 15.59%

m/z—> 5000

— 20 41 —ll—ull —LI 40 55

60 70

80 84

98 112 127 100 120 140 160 180 200 T J teAoblmalukoyap rl 1 1 1 1 I 40.00 40.20 40.40 40.60

08425 .D SCAN020418.M Thu May 02 15:28:12 2002 Page 13

NYC-WTC_000048164

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