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GCMS analysis results for sample AE08425, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 12 Benzoic acid, p-anilino-, m.. Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 40.44 0.33 ug/1 563459 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 37 2 1-Phenyl-3-[bis(methoxycarbonyl)... 286 C17H18O4 1000112-84-0 35 3 Benzoic acid, 3-(phenylamino)-, ... 227 C14H13NO2 055622-43-0 28 4 Silicic acid (H6-Si2-O7), hexame... 258 C6H1807Si2 004371-91-9 25 Abundance Scan 6358 (40.436 min): 08425. D (-6350) (-) m/z 227.20 100.00% 217

5000 113 40

84 98 198 , 40.20 40.40 40.60 40.80 ■ ■ i' ■ ■111 66 94744425137 151169TTU————n)mOTTT m/z 113.60 37.23% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #89099: Benzoic acid, p-anilino-, methyl ester 217 196

5000 ■ ■ i ■ • T ' ' 40.20 40.40 40.60 40.80 167 m/Z 40.10 26.82% 51 65 77 98 115 139 180 1 1 i ■ " ' rd* 1 11 1 i1 1.... 1 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #89072:1 -Phenyl-3-[bis(methoxycarbonyl)methyl]hex-1 -en-4-yne 155 2.7

59 115 40.20 40.40 40.60 40.80 167 m/z 226.20 24.44% 5000 71 91 128

. 195 211 .. 111193. , 141 l’ , ..171 L 286 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #89078: Benzoic acid, 3-(phenylamino)-, methyl ester A 217 40.20 40.40 40.60 40.80 m/z 228.10 18.52%

5000 167 196 52 64 77 98 115 139 । /z—> "I I’Htti .......... 40 60 80 182— I I I T| , I I I I' ! I I I | / 100 120 140 160 180 200 220 240 260 280 • ■ i • • 40.20 40.40 40.60 40.80

08425.D SCAN020418 .M Thu May 02 15:28:12 2002 Page 14

NYC-WTC_000048165

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NYC-WTC_000048165Source: NYC Law Department, mirrored locally

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