GCMS analysis results for sample AE08425, May 2002

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Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048148–000048168

Folder label: “GCMS X 4/9/02 A 4/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 13 Bis(2-ethylhexyl) phthalate Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 40.52 0.23 ug/1 402736 Chrysene-dl2 39.93 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Bis (2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 64 2 m-Tolyl isothiocyanate 149 C8H7NS 000621-30-7 50 3 Benzene, l-isothiocyanato-2-methyl- 149 C8H7NS 000614-69-7 50 4 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 50 Abundance Scan 6373 (40.524 min): 08425.D (-6367) (-) m/z 40.10 100.00% 43 149

5000 167 57 71 93 112 132 207 227 279 40,20 40.40 40.60 40.80 j" ।, al । | । , "11 1,1174 141 , ft , I________ I 1__ m/ Z 149.00 94.17% 11 1 ' ‘I I ' ' 1 ' I 11 rr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66784: Bis(2-ethylhexyl) phthalate 149

5000 A444q4daAaLMApAH++ 57 40.20 40.40 40.60 40.80 167 43 71 m/z 167.00 30.49%

m/z-> ...... L., —4. T 132 | 113 ' I' ' 1 1 I 1 11 1 I ' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 279 1 ■ ■ 1 1 A Abundance #66834: m-Tolyl isothiocyanate 149 91 A’ A I j r1-' 444— 40.20 40.40 40.60 40.80 5000 m/z 57.10 23.08%

m/z~> 39 26 ..8 1’10*—1*0/00 65 52,78 1 104117 133 I'. 0000tnTammm)muOPTTT — "131 11111 T7u "III T ii ETTI 20 40 60 80 100 120 140 160 180 200 220 240 260 280 wltulwppnd Abundance #66916: Benzene, 1 -isothiocyanato-2-methyl- 149 40.20 40.40 40.60 40.80 m/z 41.10 20.27%

5000 117 91 65 J | 78 | 104 . 133 , ............ .................. ......... .............. —rr । ■ 1 ■ ■ । ■ 1 ■ • • - । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 40.20 40.40 40.60 40.80

08425.D SCAN020418 .M Thu May 02 15:28:13 2002 Page 15

NYC-WTC_000048166

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