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GCMS chain of custody form, sample AE10236, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10236 on May 20, 2002, including surrogate compound data.

NYC-WTC_000024366–000024379

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024378
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020509\10236.D Vial: 14 Acq On 9 May 2002 11:28 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 Di-n-octyl phthalate Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

40.52 0.34 ug/1 37625 Chrysene-dl2 39.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual y7 $ 1Din - U d Cy 1 phthalate 390 C24H3804 000117-84-0 72 Bis(2-ethylhexyl) phthalate 1 0. 12 390 C24H3804 000117-81-7 45 3 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 42 4 Di-n-octyl phthalate 390 C24H3804 000117-84-0 40 Abundance Scan 6372 (40.518 min): 10236.D (-6366) (-) m/z 149.00 100.00% 149 J

57 5000 41 113 167 84 132 186 229 279 329 40.20 40.40 40.60 40.80 ’ 41’ - -- m/z57.00 51.91% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #123444: Di-n-octyl phthalate 149

5000 41 57 Al Ma, , AMALHa 40.20 40.40 40.60 40.80 167 m/z 43.10 41.02% UUI 1A9sp -ITIr 113 132 191 279 261 I

Wull ' i' ‘ " i' ■'' i “ " i1" ' i ■' ■ ■ 11 “ ■ i' ■ " i ‘ ■ miz- > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #66784: Bis(2-ethylhexyl) phthalate 149 > ■ i • ■ 40.20 40.40 40.60 40.80 5000 m/z 70.10 35.87% 57 167

miz-> .. 111, 1.1132TTmtmmOTDumOTTTT 83 113 r111111111 r11111 , ,

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 279

Abundance #66787: Phthalic acid, diisooctyl ester 149 40.20 40.40 40.60 40.80 m/z 41.00 35.71%I 5000 57 167

41 I 83 132 ................................... M 113 | " i1'111 ■"' i1" ' ।'11 ■ । ■ ■ ■ ■ ।r"1111" i1"11'1' rrn 11111 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 | 40.20 40.40 40.60 40.80

10236.D SCAN020507.M Tue May 14 14:24:01 2002 Page 9

NYC-WTC_000024378

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NYC-WTC_000024378Source: NYC Law Department, mirrored locally

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