GCMS chain of custody form, sample AE10236, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020509\10236.D Vial: 14 Acq On 9 May 2002 11:28 pm Operator: Nefliu Sample sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.36 ug/1 46164 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene -d10— 001719-06-8 72 188 C14D10 2Phenanthreno - dl 0 001517-22-2 43 188 C14D10 3 2-Methylinden-3-one carboxylic acid 188 C11H8O3 1000214-94-6 32 4 Antipyrine 188 C11H12N20 000060-80-0 32 Abundance Scan 4914 (31.952 min): 10236.D (-4904) (-) m/z 188.20 100.00% 188

5000 80 94 160 ,.......... 42 '|52li i ! । n66li | n ll' i il > । I| IL । । | H i | | | | i r[n li 41 ii 112121 i 31.60 31.80 32.00 32.20 TITTTTTTTTTTTTTTT111’ m/z .94.10 30.45% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d ID- 188

5000 31.60 31.80 32.00 32.20 m/z 80.00 29.94% 80 94 160 , |. 66

n/z-> 17 30 42 52 146—4.179179 108118 132 ' 1 | > < > । | 1 । • 1 | I I I -HHH ' ■ I"111" " i" " 1111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d1 0 188 ■ • | ■ r l ■ • ' T | 1 1 | > 1 ■ 1 | 31.60 31.80 32.00 32.20 5000 m/z 184.10 24.76%

80 94 160 30 42 52 66 TIWWWImWTmTTTTTTHH 1 .108118 132 146 | 170179 TTTTt ‘p-rrr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79734:2-Methylinden-3-one carboxylic acid 1(18 31.60 31.80 32.00 32.20 ' m/z 160.10 21.57% 115 5000 160 63 89 132 143 104 170 51 11" " ।"" ।" " ।1 ■" |T TPTTTT TUT ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

10236.D SCAN020507.M Tue May 14 14:23:59 2002 Page 8

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