GCMS analysis page for sample AE11570, May 2002

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Data File : C:\MSDCHEM\1\DATA\020521\11570.D Vial: 23 Acq On : 22 May 2002 6:05 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.34 ug/1 33502 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual -1 Anthracene - dl 0 - 188 C14D10 001719-06-8 42 2 Phenanthrene -diO 188 C14D10 001517-22-2 42 3 Benzaldehyde, 2,6-difluoro-4-hyd... 188 C8H6F2O3 1000116-28-9 12 4 Benzenesulfonamide, 3-amino-4-hy. . . 188 C6H8N2O3S 000098-32-8 9 Abundance Scan 4914 (31.952 min): 11570.D (-4910) (-) m/z 188.20 100.00% 188

5000 94

49 64 78 108 158 31.60 31.80 32.00 32.20 265 O-TT —H—HL -'I... 1 / .................... |........ I m/z 94.20 43.09% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #79826: Anthracene-d1 0- _/ 188

5000 31.60 31.80 32.00 32.20 m/z 187.10 28.78% 80 94 160 28 40 52 66 n/z-> 0 — 20 40 60 —10118 13246 — 1 ■ i 1 ' 1 ' i ■ ■ ■ 1 i ■ • 80 100 120 140 160 180 200 220 240 260 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 100.10 13.31%

80 94 160

n/z—> 0- ,12849566.1., 20 40 1 108120132 146 11 TTTTTTTT 4.A. 60 80 100 120 140 160 180 200 220 240 260 ‘ I ' 1 ' ' 1 1 ' 1 1 1 1 1 - Abundance #79823: Benzaldehyde, 2,6-difluoro-4-hydroxy-3-methoxy- 188 31,60 31.80 32.00 32.20 m/z 184.05 13.31% 5000 173 43 57 69 83 97 117 145 /....................................... O—) +-41-4444allul+————.4+131—199— 1 ' i ■ ' ' 1 i 1 ‘ 1 1 i ■ r n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 31.60 31.80 32.00 32.20

11570.D SCAN020521.M Fri May 24 09:48:55 2002 Page 5

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