GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10133 on May 17, 2002.

NYC-WTC_000046180–000046191

Folder label: “GCMS X 5/7/02 A 5/14/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10133.D Vial: 20 Acq On : 14 May 2002 7:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 . M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 37959 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 001719-06-8 90 188 C14D10 2 Phenanthrene-d10 001517-22-2 72 188 C14D10 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 38 Abundance / Scan 4915 (31.958 min): 10133.D (-4905) (-) m/z 188.15 100.00% 188

5000

———————————— 80160 94 31.60 31.80 32.00 32.20 42 51 66 113 136 TUTTTITTTTTTTTTH I'll.|il.... TTTERTnunT | TTHp 173 ‘ 0 m/z 189.30 15.14% n/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 1T | .. I I | I I I , | I 31.60 31.80 32.00 32.20 m/z 94.10 15.01% 80 94 160 , . 66 17 30 42 52 nIu0——000———urttr HTHH 108 118 132 I I I I I I [ I I I I I 1 I I I I 1'1 I 146—44179179—. TT r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1f8 / 31.60 31.80 32.00 32.20 5000 m/z 184.10 13.35%

80 94 160 30 42 52 66 , | 108 118 111111 r111111" i"1 Ttti 11 ii111 ui i |. 11. । I I । r 111 i 11 11 r i [ । i 11 11 i । TTT 132 146—4179179— ‘T m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 50 160 170 180 190 Abundance #79771: 3-Amino-4-methyl-6-methoxyquinoline 188 31.60 31.80 32.00 32.20 m/ z 80.20 12.63% 145 5000

117 1 30 41 51 63 77 89 102 159 173 m/z-> JU 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 rir|'i i I i I’ i i | I r - 31.60 31.80 32.00 32.20

10133.D SCAN020507.M Wed May 15 08:28:53 2002 Page 6

NYC-WTC_000046189

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GCMS analysis results, sample AE10135, May 2002 · Box DEP Box 25

NYC-WTC_000046192

Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.

1 shared topics · Same agency, volume and box · similarity 0.997