GCMS analysis results for sample AE11279, May 2002

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Data File : C:\MSDCHEM\l\DATA\020515\11279.D Vial: 13 Acq On : 15 May 2002 11:40 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.38 ug/1 41263 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual Anthracene-d10- 188 C14D10 001719-06-8 80 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N20 1000213-71-3 47 3 2,6 Naphthoquinone, 1,5-diamino- 188 C10H8N2O2 002783-59-7 43 4 Pen acyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H2Q 1000215-61-8 42 Abundance Scan 4914 (31.952 min): 11279.D (-4905) (-) m/z 188.20 100.00% 188

5000 80 158 31.60 31.80 32.00 32.20

mz-> ' ' 1 I 1 1 1 ‘ I ' 50 100 132—144 200 438 1 ‘ 1 m/z 80.05 30.76% 150 250 300 350 400 Abundance #79826: Anthracene-d1 0- 188

5000 ..1 9* l r T ! I | > I I I | I 31.60 31.80 32.00 32.20 m/ Z 187.10 17.20% p 94 160 , 17 .42466411. 132.1 1 , 1 11 I™ 1 1 ’ 1 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188

145 31.60 31.80 32.00 32.20 5000 m/z 158.00 16.28%

41h t 63 89 117 - * shh - m "4 • " I /z-> 50 100 150 200 250 300 350 400 Abundance #79755:2,6-Naphthoquinone, 1,5-diamino- । r.. >I ,,, t-| । , 188 31,60 31.80 32.00 32.20 m/z 76.00 13.80% 132 5000 160 66 104 , 4 A 4 . h 1 1.. m/z—> 50 100 150 250 300 350 400 31,60 31.80 32.00 32.20

11279.D SCAN020507.M Thu May 16 14:41:27 2002 Page 6

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