GCMS analysis results for sample AE11279, May 2002

NYC 9/11 Public Portal Document Llbrary searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11279.D Vial: 13 Acq On : 15 May 2002 11:40 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

31.08 0.30 ug/1 32770 Phenanthrene- dl 0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-HydWxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 47 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 47 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 47 4 Anthracene, 1-methyl- 192 C15H12 000610-48-0 40 Abundance / Scan 4766 (31.082 min): 11279.D (-4754) (-) m/z 192.10 100.00% 192

5000

82 146 b. 30.80 31.00 31.20 31.40

nlz-> 140,11,11,4/127,1,.... , 50 100 150 —T 200 250 300 350 400 450 506 500 m/z 146.20 27.95% Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 .... .0 30.80 31.00 31.20 31.40 63 89 . m/z 191.00 24.60% tl ,i145 J u 4 ,i. Ji, .117 mfz-> 50 'T i 100 ■ t. . 1 ■ ■ 150 r ■ ' ■ 200 ■ । 250 ■ 1 1 300 ■ । 350 ■ _____ ■ ■' । ■ 1 1 ■ । ■ ' ' ■ । ■ ■ ' ■ । ■ ■ • ' । ■ ■ 400 450 500 V Abundance #125847: Anthracene, 2-methyl- 192 . ..... f u.... . 30.80 31.00 31.20 31.40 5000 m/ z 81.90 16.99%

28 63 96i 20 139 165 | JI 4 n 1 r ddn" t ~ t i 'i J* । । 11 n । !■ । ■ j । । । । । > । । । । । । । । । ) । j । 1 nz-> 50 100 150 200 250 300 350 400 450 500 Abundance #125845: Anthracene, 2-methyl- 192 30.80 31.00 31.20 31.40 m/z 193.20 16.29% 5000

74 % 11 1 I"T"I । ■ । -i i 13915 /z—> 50 100 150 200 250 300 350 400 450 500 30.80 31.00 31.20 31.40

11279.D SCAN020507.M Thu May 16 14:41:26 2002 Page 5

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