GCMS analysis results for sample AE11279, May 2002

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Data File : C:\MSDCHEM\l\DATA\020515\11279.D Vial: 13 Acq On : 15 May 2002 11:40 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.45 0.56 ug/1 54453 Naphthalene-d8 16.53

J it# of 5

Cyclopentasiloxane, decamethyl- 2 Cyclopentasiloxane, decamethyl- Tentative ID

3 Benzoic acid, 2- (trimethylsilyl ... 282 370 370 MW MolForm

C10H3005Si5 C10H3005Si5 C13H2203Si2 CAS#

000541-02-6 50 000541-02-6 40 003789-85-3 32 Qual

4 Benzoic acid, 2- (trimethylsilyl... 282 C13H2203Si2 003789-85-3 32 Abundance Scan 2106 (15.453 min): 11279.D (-2098) (-) m/z 73.10 100.00% 73

5000 267 355 . . ( t . . -r q । . a > -i'i-i । t । i" । 48 15.20 15.40 15.60 15.80

mlz-> . irMliti "I "I""| 125 3394—— I " " I" "I • ■ 179 , 207 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 l | 249 I | v Mi I'll ' I " 1 ■ i" " i1' m/z 355.00 29.27% Abundance #115315: Cyclopentasiloxane, decamethyl- 73

5000 267 355 -1 15.20 15.40 15.60 15.80 m/ z 2 67.00 26.53% 45 191207223 251 323339 I 'I‘ ' I ' " ’ I' 1 D । । । । । j । i 11 । । < • । । «i > । ।»11 i 11 rrq 11 IIIIIIIdupu TIIPWTTTTTT 1‘T m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 A ... 1.... . 15.20 15.40 15.60 15.80 5000 267 m/z 74.10 14.45% 355 45

iz-> 28 1 1 96 115133149165 96 115 11'1 ‘ i'1" i" r ' ‘' i " '11" " i ■ 133149165, , 193 223 ... i' " 11 * Ti l r. ■ । । i i ri । i rT i । I. I I I I I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 307323339 111" " 1'" 1' 1"

Abundance #115268: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... ' 1 1 1 1 1 ' i ' A.. | I ■ ' i ■ ■ ■ 1 i • ■ 73 15.20 15.40 15.60 15.80 m/ Z 2 68.10 10.57%

5000 267

45

m/z—> 28.4 1, 91.115 135151. 175 193209.233249 . ′ j < <l > । > > > i | । > i । > vi > ] > > । । ! । > < ■ । । । > । ! ■ i f i । i r i i । ‘Ti i । i i i i । i i i i । i i i i । i i i i । i । 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 15.20 15.40 15.60 15.80

11279.D SCAN020507.M Thu May 16 14:41:26 2002 Page 4

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