GCMS analysis results for sample AE11304, May 2002

NYC 9/11 Public Portal Document Llbrary searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.95 0.33 ug/1 25995 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

. 1 Anthracene-dlO- 188 C14D10 001719-06-8 50 2 Pertacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 36 3 Benzene, 2-butyl-1,3,4-trifluoro- 188 C10H11F3 022872-43-1 9 4 Phenanthrene-diO 188 C14D10 001517-22-2 9 Abundance Scan 4914 (31.952 min): 11304.D (-4906) (-) m/z 188.20 100.00% 188

5000

80 94 44 66 156 31.60 31.80 32.00 32.20 qmpppl 11111 ii I, । n 11 — I " " 11111 1 11 "111 1 |rl" " I'1" I — m/z 94.20 23.02% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 ■ । । । ' ' * i । । ‘ ^ । ■■ > > ' I > 1 । । I • 31.60 31.80 32.00 32.20 80 94 m/z 80.30 18.68% 66 160 ,i.

m/z-> 17 30 42 52 ‘f ■ i> 11'' • > i11 ‘' 11' ‘1111' mH 108 118 > • i > । • > i • । • 111 > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132.146,4-170179l,—4 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... 188 /................................ 31.60 31.80 32.00 32.20 5000 79 91 m/z 156.10 14.99% 55 67 105 117 131

mlz-> ...................... ...... 11' " ‘ I'1" 11" ‘ I'1" /’’’’11 145158.173.. Il I 1111! rri I I'l 11 1111-I'111., 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #8892: Benzene, 2-butyl-1,3,4-trifluoro- . . । r. . i~rr । ITPrT । । । -|-i । । । । । 43 145 31.60 31.80 32.00 32.20 m/z .66.10 13.12% 188 5000

29 63 75 87 99 119,132 159 TI—‘"UIEEIIF"E"TIT*—dROgTTRTTegT —TP pTTT /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

11304.D SCAN020507.M Fri May 17 13:11:26 2002 Page 10

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