GCMS analysis results for sample AE11304, May 2002

NYC 9/11 Public Portal Document Llprary searcn compound Report

Data File : C:\MSDCHEM\l\DATA\020516\11304.D Vial: 15 Acq On : 16 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 9 1,2,3,4-Cyclopentanetetrol,... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 34.91 0.28 ug/1 22126 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 3,4-Cyclopentanetetrol, (l.a... 134 C5H10O4 014003-71-5 10 2 3 hylheptanoic acid 158 C9H1802 014272-47-0 10 3 Butyraldehyde, semicarbazone 129 C5H11N30 013183-21-6 9 4 Octanoic Acid 144 C8H16O2 000124-07-2 9 Abundance Scan 5417 (34.907 min): 11304.D (-5408) (-) m/z 73.00 100.00% 60 73 43 85 5000 97 129 34.60 34.80 35.00 35.20 36 ■ ' I ■ ' ' ' i ' 1 ' 1 i ‘ ‘ ' i ■ ■ • ■ i ■ • T 1 •1111111111ITET .. ।.... । . 11. ■ m/z 60.10 89.93% 10 20 30 40 50 80 90 100 110 120 130 n/z-> Abundance 60 70 #25804:1,2,3,4-Cyclopentanetetrol, (1.alpha.,2.beta.,3.be... 60 73 I 98 5000 44 ■ l • * ■ ■ I 34.60 34.80 35.00 35.20 m/z 57.20 84.90%

m/z-> ................... rl 1 1 1 111 lTr 111111 ' 10 i 20 30 i p 40 +4544 1 66.1181 488— 1 199.1.111 130 50 60 70 80 90 100 110 116

120 Abundance #16943:3-Ethylheptanoic acid

41 57 1 ■ i ' ■ I ■. 11 I ' ( ' 1 1 1 1 1 1 1 1 34.60 34.80 35.00 35.20 5000 29 m/z 43.20 78.83% 69 98 83

mz-> ' ' i ■ 10 15 +4445 L 20 30 40 50 60 70 —+ 80 90 100 — 111 110 120 129

130 Abundance #20135: Butyraldehyde, semicarbazone 6b 34.60 34.80 35.00 35.20 m/ Z 69.00 61.21% 5000 43 71

129 86 101

n/z—> 1 * । 1 1 1 1 i 1 1 1 ' 1 1 1 1 1 r 10 20 30 40 +t 50 60 —I 70 +9— 80 90 100 114 ■ - I ■ 1 '"' i । । । i'| । । ।

110 120 130 34.60 34.80 35.00 35.20

11304.D SCAN020507.M Fri May 17 13:11:28 2002 Page 11

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