DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document

Llprary Searcn Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\0201B.D Vial: 1 Acq On : 27 Feb 2002 10:33 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Cycloheptanone, 4-phenyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.78 0.61 ug/L 458992 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cycloheptanone , 4-phenyl- 188 C13H160 067688-28-2 43 2 1,4-DIMETHYL-5-PHENYL-4 -IMIDAZOL. . . 188 C11H12N2O 022199-48-0 40 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 38 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 37 Abundance Scan 1719 (Z2.779 min): 0201 B.D (-) m/z 188.10 100.00% 188

5000

94 132 158 22.40 22.60 22.80 23.00 23.20 44 52 66 ,। > l ] ‘ ' 1 । f । । | । । 1 1 | । 1 I I | 1 " I' | ' "'I |'l । L m/ z 94.05 20.70% 0! 1111111111 '■ i111 ■ i'11H11" i1 ...................................................................... | ' ■ ■ ■ | I 1’1 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98298: Cycloheptanone, 4-phenyl- US 117 104 160 -- 5000, 131 170 22.40 22.60 22.80 23.00 23.20 145 m/z 189.10 10.10%

0 '' I 1 1 11 111'' I''1 1 I'1 '' I'1111''1' I' 111111 11m Tr L m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #97863:1,4-DIMETHYL-5-PHENYL-4-IMlDAZOLIN-2-ONE $$ 2H-Imi... 188 .. n...... 22.40 22.60 22.80 23.00 23.20 5000 m/ z 80.00 9.26% 118 77 105 130 144 159 173 0 .................................... Il l 11111' ■ i'1111 ■1‘■i11 ■ ‘ i''1 ’ i1'111■1'11 ■r 11 1’ _L pl..... ............... 1 Ilr m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 — Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 22.40 22.60 22.80 23.00 23.20 m/z 184.00 8.67%

5000

80 94 66 158 —— - ■ i ■ ■ ■ ‘ । ■ i ■1 ■ ■ i ■ ■ ■11 ■ ■' ■ i ■'1 'I' ■ " i'1 0 TTITTTTIWTTITTTTT T-t-T ■m-rf m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

201B.D HP022102.M Thu Feb 28 08:46:40 2002 Page 11

NYC-WTC_000004959

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999