GCMS quantitation results for sample AE10301, May 2002

NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10301.D Vial: 24 Acq On : 17 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 15.46 0.30 ug/1 19183 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 C#clopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 38 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 28 Abundance Scan 2107 (15.459 min): 10301 .D (-2099) (-) m/ z 73.10 100.00%| 73

5000 267 355 15.20 15.40 15.60 15.80 i. 191.......... L.................. I,.............. m/z 355.00 L T 33.74% Tl/Z-> 50 100 150 200 250 300 350 400 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 .................... 5000 1 ' I ■ 1 ' ' ' I ' ' 1 ' I ' ' 15.20 15.40 15.60 15.80 m/ z 2 67.00 28.66% 45 TT ,.. .207* mlz-> 50 100 150 200 250 300 350 400 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

15.20 15.40 15.60 15.80 5000 267 m/ z 268.00 12.16% 355 45 . .1 1 96 133 165,193 223 247 1 293 323 --—1 ' 1 ■ i ' ■ 1 ■ i "■ ■' ■ ‘* I AII mlz—> 50 100 150 200 250 300 350 400 Abundance #27959: Noradrenaline tetraTMS 73 15.20 15.40 15.60 15.80 m/z 355.90 11.04%| 5000 102 355

45 | 1 147 I 442 TI ■ i n/z—> 50 100 150 200 250 300 350 400 15.20 15.40 15.60 15.80

10301.D SCAN020507.M Fri May 17 10:51:27 2002 Page 5

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