Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050222–000050239Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31645.D Vial: 1 Acq On : 22 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamet... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.09 ug/L 38938 Naphthalene-d8 13.19 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 3 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 32 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 32 Abundance Scan 803 (12.542 min): 31645.D (-) m/z 73.10 100.00% 73
5000 267 355 ■ ■ i ‘ ' 1 ■ i 1 ■ • • i 1 1 ' 1 I ' ' 1 ' 1 ' 12,20 12.40 12.60 12.80 40 ... nz-> ■ • i 50 100 1 150 200 250 300 350 400 m/z 267.00 38.95%
Abundance #313065: Cyclopentasiloxane, decamethyl- 73
500) 267 • > i ■ • • • । ■ 1 i ■ • ■ ■ i ■ ■ ■ ■ i 1 12.20 12.40 12.60 12.80 355 m/z 355.10 36.08% 45 — 193 iz-> 50 ‘I * • • ///dB* 1 I • 100 150 t
200 250 223— 300 323 —IT 350 400 T
Abundance #313068: Cyclopentasiloxane, decamethyl- 73 T T-* 355 12.20 12.40 12.60 12.80 267 m/z 267.90 10.53% 5000
.............................. 207 — 323 , ’ * i TT nn—nn—1. T miz—> 50 100 150 200 250 300 350 400 Abundance #357156: Noradrenaline tetraTMS T T T I ' • ■ ■ i 1 73 12.20 12.40 12.60 12.80 m/z 356.10 9.96%
5000 102 355
45 147 442 i" 1 1 • TI—9—————9—1—m—-—=—T=1 ■ i ■ ■ i ■ ■ ■ ■ i ■ ■ J****I*’11 m/z—> 50 100 150 200 250 300 350 400 12,20 12.40 12.60 12.80
31645.D SCAN508.M Thu Jan 24 13:50:35 2002 Page 8
NYC-WTC_000050233
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NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050240
Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder