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← Document results/DEP Box 28/GCMS X 1/3/02 A 1/22 - 1/23/02
Document / 18 pages

GCMS analysis results for sample AD31645, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050222–000050239

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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Scanned page image, NYC-WTC_000050234
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31645.D Vial: 1 Acq On : 22 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 IH-Azonine, octahydro- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.09 ug/L 42520 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual l IH-Azonine, octahydro- 127 C8H17N 005661-71-2 4 NO 2 N-Carboethoxyimidazole $$ 1-Carb. . . 140 C6H8N2O2 019213-72-0 3 C009 3 Methyl 2-Methylenecyclopentaneac... 140 C8H12O2 000000-00-0 2 . 4 2-Methyl-3-methoxy-4H-pyran-4-one 140 C7H803 000000-00-0 2 CV Abundance Scan 876 (13.375 min): 31645.D (-) m/z 140.00 100.00% 1-0

5000

70 40 84 94 13.00 13.20 13.40 13.60 13.80 ■ i ■1' ‘ i ■ ■ ■ ■ i ■ ■'11 ■ • ■ ■ i ■ ■ ......11.,.11.,..I. TI m/z 70.10 17.59% z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #23801:1 H-Azonine, octahydro- 33 56

70 5000 ‘ *‘**I* 1300 13.20 13.40 13.60 13.80 42 84 127 m/z 94.10 12.10% 96 — ' * । ’ * i • • I8* TI—nnI,I—m112—B—uegeu; miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35163: N-Carboethoxyimidazole $$ 1-Carbethoxyimidazole $$... 23 68

40 13.00 13.20 13.40 13.60 13.80 5000 m/z 84.00 11.21% 81 140

rrTr TIr Iu—nr 54 ■ ■ ।11 ■11. ■ I ,.... T95........ . ‘ I miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35861: Methyl 2-Methylenecyclopentaneacetate TTTr j 1 1-0 13.00 13.20 13.40 13.60 13.80 109 m/z 96.10 10.37%

5000 41 57 79 ‘ i ■ ■ ■ ■ i ‘ ■ ■ ■ i • ■ ■ ' i '' ■ ■ i ■•‘■i‘‘'i■•‘•i•■■■i‘‘11'■■ • 111111'1 '1 1 ‘ I ■ i ' 1 1 ■ i ■ • ■ ‘ i ■ n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

31645.D SCAN508.M Thu Jan 24 13:50:35 2002 Page 9

NYC-WTC_000050234

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NYC-WTC_000050234Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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