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← Document results/DEP Box 28/GCMS X 1/3/02 A 1/22 - 1/23/02
Document / 18 pages

GCMS analysis results for sample AD31645, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050222–000050239

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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Scanned page image, NYC-WTC_000050235
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31645.D Vial: 1 Acq On : 22 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 8-(3-Hydroxyethyl)-3-methox... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 18.72 0.06 ug/L 29506 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 8-(3-Hydroxyethyl)-3-methoxybicy... 192 C12H16O2 000000-00-0 9 2 Propanoic acid, 2-chloro- 108 C3H5C102 000598-78-7 9 3 Ethyl Chloride 64 C2H5C1 000075-00-3 7 4 Ethyl Chloride $$ Ethane, chloro... 64 C2H5C1 000075-00-3 7 Abundance Scan 1344 (18.718 min): 31645.D (-) m/z 64.00 100.00% 64 192

5000 128 ... .............. /.................... 160 180 49 18.40 18.60 18.80 19.00U ।■. •. । ■ ■ ■.।। ■ •. t" ’ I B11 m/z 191.80 98.84% mz-> 2030405060 70 8090 100110120130140 150 160 170 180190 200 Abundance #103293:8-(3-Hydroxyethy!)-3-methoxybicyclo[4.2.O]octa-1,... 161 192 147

103 121 5000 131 177 T T T T 18.40 18.60 18.80 19.00 m/z 128.00 33.60%

miz—> .. ।.... ।।....।....।....।.... ।....।.... ।.... ।..., ।..., ।.. 2030405060 70 8090 100110 120130140 150 160 170180190 200 LH ... 1*** 'T

Abundance #11024: Propanoic acid, 2-chloro- 27 64 T T T 18.40 18.60 18.80 19.00 5000 45 m/z 193.80 26.25% N 73 08 ■ ! I1.।।1 (।|।11 i. 11... i ।... 11।।. ■11'1 miz—> 20 30 40 50 60 70 80 90 100110 120 130140 150160 170 180190 200 Abundance #930: Ethyl Chloride 64 18.40 18.60 18.80 19.00TT 29 m/z 160.00 23.28%

5000 49

n/z—> •111 • m 112111111611117110/1121111021/1001122110011211711101113011101117 2030405060 70 8090 1(X) 110 120 130 140 150 160 170 180 190 200 • • I 1 ’ ’ ‘ I ‘ ‘ 4 * I • ‘ 1 ‘ I • ‘ 18.40 18.60 18,80 19.00 ‘ I

31645.D SCAN508.M Thu Jan 24 13:50:35 2002 Page 10

NYC-WTC_000050235

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NYC-WTC_000050235Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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