Laboratory report documenting GCMS analysis of sample AD31645 with detection of unknown compounds and surrogate recovery.
NYC-WTC_000050222–000050239Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31645.D Vial: 1 Acq On : 22 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 8-(3-Hydroxyethyl)-3-methox... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 18.72 0.06 ug/L 29506 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 8-(3-Hydroxyethyl)-3-methoxybicy... 192 C12H16O2 000000-00-0 9 2 Propanoic acid, 2-chloro- 108 C3H5C102 000598-78-7 9 3 Ethyl Chloride 64 C2H5C1 000075-00-3 7 4 Ethyl Chloride $$ Ethane, chloro... 64 C2H5C1 000075-00-3 7 Abundance Scan 1344 (18.718 min): 31645.D (-) m/z 64.00 100.00% 64 192
5000 128 ... .............. /.................... 160 180 49 18.40 18.60 18.80 19.00U ।■. •. । ■ ■ ■.।। ■ •. t" ’ I B11 m/z 191.80 98.84% mz-> 2030405060 70 8090 100110120130140 150 160 170 180190 200 Abundance #103293:8-(3-Hydroxyethy!)-3-methoxybicyclo[4.2.O]octa-1,... 161 192 147
103 121 5000 131 177 T T T T 18.40 18.60 18.80 19.00 m/z 128.00 33.60%
miz—> .. ।.... ।।....।....।....।.... ।....।.... ।.... ।..., ।..., ।.. 2030405060 70 8090 100110 120130140 150 160 170180190 200 LH ... 1*** 'T
Abundance #11024: Propanoic acid, 2-chloro- 27 64 T T T 18.40 18.60 18.80 19.00 5000 45 m/z 193.80 26.25% N 73 08 ■ ! I1.।।1 (।|।11 i. 11... i ।... 11।।. ■11'1 miz—> 20 30 40 50 60 70 80 90 100110 120 130140 150160 170 180190 200 Abundance #930: Ethyl Chloride 64 18.40 18.60 18.80 19.00TT 29 m/z 160.00 23.28%
5000 49
n/z—> •111 • m 112111111611117110/1121111021/1001122110011211711101113011101117 2030405060 70 8090 1(X) 110 120 130 140 150 160 170 180 190 200 • • I 1 ’ ’ ‘ I ‘ ‘ 4 * I • ‘ 1 ‘ I • ‘ 18.40 18.60 18,80 19.00 ‘ I
31645.D SCAN508.M Thu Jan 24 13:50:35 2002 Page 10
NYC-WTC_000050235
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NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050240
Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050258
Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051024
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 8-10, 2002 testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050354
Laboratory report for sample AE00100 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050276
Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050370
Laboratory report for sample AE00101 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050177
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050178
Instrument log sheet recording sample counts and operational parameters for GCMS Method 508 analysis in January 2002.
Filed in the same folder
NYC-WTC_000050180
Calibration report for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050184
Reference scan data for GCMS analysis of sample AD31647 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
Filed in the same folder