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GCMS analysis results for sample AE00614, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.

NYC-WTC_000051605–000051623

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4 :17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamet... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.11 ug/L 78789 Naphthalene-d8 13.19 Hit# Of 5 Tentative ID MW MolForm , CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 42 3 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 37 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 Abundance Scan 803 (12.541 min): 00614.D (-) m/ z 73.10 100.00% 73

5000 ......... .............. 267 355

12.20 12.40 12.60 12.80 45 154 193 - TTuummunUH’uommunPTTT -1 ■ ■ ■ 323 251 L 37.16% ■ i ■ ■ • • i > > T’l m/z 267.00 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12.20 12.40 12.60 12.80 m/z 355.10 35.12% , . 191207 251 J 323339 ■ ■ | ' 1 1 | ■ 1 | ' I I ■ ■ . | . I I ' . . . | . . . . | I i , | i . I , | , , , , I . . . , ( , , , , । ■T■ । । । ■ । < । TTT i’’ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ........................ 12 20 12.40 12.60 12.80 5000 267 m/z 268.00 12.23% 355 45 11 |TTIIIuupuTT 193 223 251 J " i ■'111 " 323339 j " i " " i ■ " ' I " 111'1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 12.20 12.40 12.60 12.80 m/z 356.10 11.73%

5000 355 44 11 TT91 ..... .. 130147 .. 193...... 267 ........ . , ■ 1 t ' n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

)0614.D SCAN508.M Wed Jan 30 09:02:15 2002 Page 8

NYC-WTC_000051616

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NYC-WTC_000051616Source: NYC Law Department, mirrored locally

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