GCMS analysis report sample AE10245, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020516\10245.D Vial: 21 Acq On : 17 May 2002 5:06 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 15.45 0.23 ug/1 14699 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 38 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 38 4 N- thyladrenaline, tri-TMS 413 C19H39NO3Si3 1000071-72-1 36 Abundanc Scan 2106 (15.453 min): 10245.D (-2098) (-) m/z 73.10 100.00% 73

5000 355 267 51 15.20 15.40 15.60 15.80 193 — TII m/z 355.10 41.08% m/z-> 50 100 150 200 250 300 350 400 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 15.20 15.40 15.60 15.80 m/z 267.00 37.95% 45 TI ... .271 323 m/z-> 50 100 150 200 250 300 350 400 Abundance 73 #27959: Noradrenaline tetraTMS

. A.... 15.20 15.40 15.60 15.80 5000 102 355 m/z 51.00 24.95%

45

miz-> TH 50 I ...17.. . 442 TI 100 150 200 250 300 350 400 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 15.20 15.40 15.60 15.80 m/z 267.90 18.75% 5000 267 355 45 , I I 96 133 165 193, 223 247 293 323 1 1 i 1 ■ i 1 r 1 n/z—> 50 100 150 200 250 300 350 400 15.20 15.40 15.60 15.80

10245.D SCAN020507.M Fri May 17 10:46:34 2002 Page 4

NYC-WTC_000024858